CAJ | 학술논문

建立了一种超高效液相色谱同时测定金针菇、香菇和平菇中吡虫啉、啶虫脒和多菌灵农药残留的方法。结果表明，3种农药在O．02-0．50mg／L的浓度范围内呈良好的线性关系，线性相关系数为0．9998-0．9999，检出限0．0057-0．0200mg／kg，定量限小于O．059mg／kg，方法平均添加回收率在97％～108％，RSD小于13％，结果较为理想，方法简单、快速、准确。
건립료일충초고효액상색보동시측정금침고、향고화평고중필충람、정충미화다균령농약잔류적방법。결과표명，3충농약재O．02-0．50mg／L적농도범위내정량호적선성관계，선성상관계수위0．9998-0．9999，검출한0．0057-0．0200mg／kg，정량한소우O．059mg／kg，방법평균첨가회수솔재97％～108％，RSD소우13％，결과교위이상，방법간단、쾌속、준학。
A method was developed for simultaneous determination of imidacloprid,acetamiprid and carbendazim in flammulina velutipes, lentinus edodes and pleurotus ostreatus by ultra performance liquid chromatography （UPLC）. The results showed that a good linearity in the range of 0.02-0.50 mg/L with the linear correlation coefficients of 0.999 8-0.999 9, detection limits were 0.005 7-0.020 0 mg/kg, quantication limits were less than 0.059 mg/kg,the average recoveries of this method were between 97% and 108% ,with relative standard deviations of less than 13% ,and the results would be better,this method was simole ,fast and accurate.