酿酒
釀酒
양주
LIQUOR MAKING
2014年
1期
21-22
,共2页
大体积进样技术%质谱分析技术%白酒中微量物质
大體積進樣技術%質譜分析技術%白酒中微量物質
대체적진양기술%질보분석기술%백주중미량물질
large volume injection techonolgy%mass spectrometry technology%trace fragrant substances of Chinese distillery
中国白酒中含有大量的香味成分和滋味成分,其中很多物质的含量极其稀少,这就给这些物质的分析工作造成了很大的困难。通常情况下为了分析这些极微量的物质,人们需要对白酒样品进行浓缩前处理,然后再利用气相色谱对浓缩样品进行分析。样品的浓缩过程是一项非常耗时耗力的工作,并且浓缩样品中含有大量的溶剂,这些物质在色谱分析中可能引起严重的分析误差,损坏色谱柱或者检测器。而大体积进样技术(LVI)则有效地避免了这些缺点。大体积进样技术可以在短时间内对分析样品进行浓缩,并且排除掉绝大多数的溶剂,从而大大提高了分析的灵敏度。将大体积进样技术和质谱分析技术联合应用,可以大大提高对白酒中极微量成分分析工作的准确性。
中國白酒中含有大量的香味成分和滋味成分,其中很多物質的含量極其稀少,這就給這些物質的分析工作造成瞭很大的睏難。通常情況下為瞭分析這些極微量的物質,人們需要對白酒樣品進行濃縮前處理,然後再利用氣相色譜對濃縮樣品進行分析。樣品的濃縮過程是一項非常耗時耗力的工作,併且濃縮樣品中含有大量的溶劑,這些物質在色譜分析中可能引起嚴重的分析誤差,損壞色譜柱或者檢測器。而大體積進樣技術(LVI)則有效地避免瞭這些缺點。大體積進樣技術可以在短時間內對分析樣品進行濃縮,併且排除掉絕大多數的溶劑,從而大大提高瞭分析的靈敏度。將大體積進樣技術和質譜分析技術聯閤應用,可以大大提高對白酒中極微量成分分析工作的準確性。
중국백주중함유대량적향미성분화자미성분,기중흔다물질적함량겁기희소,저취급저사물질적분석공작조성료흔대적곤난。통상정황하위료분석저사겁미량적물질,인문수요대백주양품진행농축전처리,연후재이용기상색보대농축양품진행분석。양품적농축과정시일항비상모시모력적공작,병차농축양품중함유대량적용제,저사물질재색보분석중가능인기엄중적분석오차,손배색보주혹자검측기。이대체적진양기술(LVI)칙유효지피면료저사결점。대체적진양기술가이재단시간내대분석양품진행농축,병차배제도절대다수적용제,종이대대제고료분석적령민도。장대체적진양기술화질보분석기술연합응용,가이대대제고대백주중겁미량성분분석공작적준학성。
Contains the flavor and taste a lot of Chinese liquor, the content of many material extremely scarce, caused great difficulties to the analysis of these substances. Normally in order to analyze the trace substance, people need to liquor samples were concentrated before treatment, and then using gas chromatography to concentrated samples analysis. The enrichment process samples is very time consuming work, and contains a lot of solvent concentration in the sample, these substances may cause serious error analysis in chromatography column, damaged or detector. While large volume injection (LVI) technology can effectively avoid these shortcomings. Large volume injection can be concentrated on the analysis of samples in a short time, and eliminate most of the solvent, thereby greatly improving the analytical sensitivity. The large volume injection technology and mass spectrometry combined with accuracy, can trace component analysis work is greatly improved in liquor.