CAJ | 학술논문

用阴极固相电解还原法，将氧化铅置于特定的阴极板上，在氢氧化钠溶液中通以直流电进行电解，对电解工艺参数进行试验。结果表明，采用阴极固相电还原法制备金属海绵铅的最佳工艺参数是：电解液中氢氧化钠浓度10％，电解温度45～60℃，电流密度600 A/m2，同极距80 m m。
용음겁고상전해환원법，장양화연치우특정적음겁판상，재경양화납용액중통이직류전진행전해，대전해공예삼수진행시험。결과표명，채용음겁고상전환원법제비금속해면연적최가공예삼수시：전해액중경양화납농도10％，전해온도45～60℃，전류밀도600 A/m2，동겁거80 m m。
The Cathode Solid Phase Electrolytic Reduction Method was used to reduce sponge lead . Electro-lytic parameter were tested by putting lead oxide onto the specific cathode plate , then connecting it with di-rect current in the sodium hydroxide solution . The best craft parameters were gotten by adopting Cathode Solid Phase Electrolytic Reduction Method to make metal sponge lead :Sodium hydroxide concentration in the electrolysis solution is 10% , electrolytic temperature is 45~60℃ , current density is 600 A/m2 , dis-tance between the same electrode is 80 mm .