CAJ | 학술논문

采用乙酸乙酯-正己烷混合溶剂（体积比为2∶1）对饮用水源地水中阿特拉津、林丹、邻苯二甲酸二正丁酯（DBP）、邻苯二甲酸二（2-乙基己基）酯（DEHP）和滴滴涕（含4种）等8种半挥发性有机物进行1次水样萃取，用气质联用法同时测定。试验表明，方法在25．0μg/L～500μg/L范围内线性良好；检出限在0．006μg/L ～0．028μg/L 之间；空白水样3个质量浓度水平的加标回收率为87．6％～109％，平行测定6次的 RSD＜5．1％；测定集中式生活饮用水源地的实际水样，未检出目标化合物，加标回收率为98．6％～109％。
채용을산을지-정기완혼합용제（체적비위2∶1）대음용수원지수중아특랍진、림단、린분이갑산이정정지（DBP）、린분이갑산이（2-을기기기）지（DEHP）화적적체（함4충）등8충반휘발성유궤물진행1차수양췌취，용기질련용법동시측정。시험표명，방법재25．0μg/L～500μg/L범위내선성량호；검출한재0．006μg/L ～0．028μg/L 지간；공백수양3개질량농도수평적가표회수솔위87．6％～109％，평행측정6차적 RSD＜5．1％；측정집중식생활음용수원지적실제수양，미검출목표화합물，가표회수솔위98．6％～109％。
The mixed solvent of ethyl acetate and hexane(V∶V=2∶1 )was used as extraction solvent to de-termine three kinds of semivolatile organic compounds in water.The compounds were impactful separated from each other through DB-1 capillary column (30 m ×0.25 mm ×0.25 μm)and then determined by GC-MS.The linearity ranged from 25.0 μg/L to 500 μg/L.The detection limits ranged from 0.006 μg/L to 0.028 μg/L.The relative bias of replicate measurements of standard solution were less than 5.1%.The average recoveries were within the range of 87.6 %~109 %.