功能材料
功能材料
공능재료
JOURNAL OF FUNCTIONAL MATERIALS
2014年
6期
6144-6147,6152
,共5页
氢氧化铟%甲苯%光催化剂%纳米材料
氫氧化銦%甲苯%光催化劑%納米材料
경양화인%갑분%광최화제%납미재료
In(OH)3%toluene%photocataly%nanomaterials
以硝酸铟为原料,六亚甲基四胺(H MT )为沉淀剂,采用一步水热法合成具有高催化活性的介孔氢氧化铟纳米晶。采用XRD、TEM、FT-IR和DRS等对样品的晶相结构、形貌和光学性能进行表征。以甲苯为模型物,测试氢氧化铟的光催化性能。结果显示其对甲苯的光催化活性要高于 TiO2(P25),且非常稳定,使用12次后其对甲苯的降解仍然可达90%。同时探讨了介孔氢氧化铟纳米晶的光催化机理。
以硝痠銦為原料,六亞甲基四胺(H MT )為沉澱劑,採用一步水熱法閤成具有高催化活性的介孔氫氧化銦納米晶。採用XRD、TEM、FT-IR和DRS等對樣品的晶相結構、形貌和光學性能進行錶徵。以甲苯為模型物,測試氫氧化銦的光催化性能。結果顯示其對甲苯的光催化活性要高于 TiO2(P25),且非常穩定,使用12次後其對甲苯的降解仍然可達90%。同時探討瞭介孔氫氧化銦納米晶的光催化機理。
이초산인위원료,륙아갑기사알(H MT )위침정제,채용일보수열법합성구유고최화활성적개공경양화인납미정。채용XRD、TEM、FT-IR화DRS등대양품적정상결구、형모화광학성능진행표정。이갑분위모형물,측시경양화인적광최화성능。결과현시기대갑분적광최화활성요고우 TiO2(P25),차비상은정,사용12차후기대갑분적강해잉연가체90%。동시탐토료개공경양화인납미정적광최화궤리。
The mesoporous nanocubes of In(OH)3 was prepared by one-step hydrothermal method using In (NO3 )3 and hexamine (HMT)as the precursor.X-ray power diffraction (XRD),UV-Vis diffuse reflectance spectroscopy (DRS),Fourier transform infrared spectrometry (FT-IR)and transmission electron microscopy (TEM)were employed to investigate the structure,morphologies,and optical properties of samples.Toluene was used as a probe molecule to investigate the photocatalytic activity of the mesoporous nanocubes of In (OH)3 .The results showed that the photocatalytic activity of the mesoporous nanocubes of In(OH)3 was more stable and higher than that of Degussa P25.The degradation rate of toluene reached 90% under UV irradiation after the In(OH)3 was recycled used for 12 times.The mechanism of high activity of the mesoporous nanocubes of In(OH)3 was also discussed.