环境科学与管理
環境科學與管理
배경과학여관리
ENVIRONMENTAL SCIENCE AND MANAGEMENT
2012年
8期
135-138
,共4页
姜春龙%顾平%陈雯雯%吕冬颖%魏庆彬
薑春龍%顧平%陳雯雯%呂鼕穎%魏慶彬
강춘룡%고평%진문문%려동영%위경빈
固相萃取%有机磷农药%气相色谱-质谱法
固相萃取%有機燐農藥%氣相色譜-質譜法
고상췌취%유궤린농약%기상색보-질보법
solid - extraction%organophosphorous pesticide%GC - MS
有机磷农药是继有机氯农药以后被广泛应用的一类农药,它对生物体具有一定毒性,因此对有机磷农药的充分提取及检测就密切关系到人们的饮食安全。传统提取底质中有机磷的方法为索式提取或者采用有机溶剂对土壤直接萃取,而本文采用亲水溶剂对土壤进行萃取,并通过固相萃取技术对其进一步纯化,气相色谱一质谱法检测,对多种有机磷农药的分离度较好。
有機燐農藥是繼有機氯農藥以後被廣汎應用的一類農藥,它對生物體具有一定毒性,因此對有機燐農藥的充分提取及檢測就密切關繫到人們的飲食安全。傳統提取底質中有機燐的方法為索式提取或者採用有機溶劑對土壤直接萃取,而本文採用親水溶劑對土壤進行萃取,併通過固相萃取技術對其進一步純化,氣相色譜一質譜法檢測,對多種有機燐農藥的分離度較好。
유궤린농약시계유궤록농약이후피엄범응용적일류농약,타대생물체구유일정독성,인차대유궤린농약적충분제취급검측취밀절관계도인문적음식안전。전통제취저질중유궤린적방법위색식제취혹자채용유궤용제대토양직접췌취,이본문채용친수용제대토양진행췌취,병통과고상췌취기술대기진일보순화,기상색보일질보법검측,대다충유궤린농약적분리도교호。
The organophosphorous pesticides, which have been widely used after the application of organoehlorine, are toxic to organisms. The extraction and monitoring of organophosphorous pesticides are closely related to the security of human health. Traditional extraction methods include Soxhlct extractor or extraction with organic solvent. This study adopts hydrophilic solvent to extract the components in soil culture and the technique of solid - extraction is used for further purification. GC - MS tests shows that this method has favorable performance for the separation of several organophosphorous pesticides.