现代农业科技
現代農業科技
현대농업과기
XIANDAIHUA NONGYE
2012年
18期
213-213,221
,共2页
底泥%多环芳烃%测定%加标回收率
底泥%多環芳烴%測定%加標迴收率
저니%다배방경%측정%가표회수솔
sediments%PAHs%determination%sample recovery
介绍运用微波萃取提取底泥中多环芳烃的技术,在优化的试验条件下,采用气象色谱—质谱法测定底泥中的16种多环芳烃,运用加标回收率验证试验方法的可行性。结果表明：采用微波消解和硅胶净化柱对样品进行前处理,方法简便,安全,样品量大,耗时短,节省溶剂,污染小,样品加标回收率为67.353%～101.666%,效果较为理想。
介紹運用微波萃取提取底泥中多環芳烴的技術,在優化的試驗條件下,採用氣象色譜—質譜法測定底泥中的16種多環芳烴,運用加標迴收率驗證試驗方法的可行性。結果錶明：採用微波消解和硅膠淨化柱對樣品進行前處理,方法簡便,安全,樣品量大,耗時短,節省溶劑,汙染小,樣品加標迴收率為67.353%～101.666%,效果較為理想。
개소운용미파췌취제취저니중다배방경적기술,재우화적시험조건하,채용기상색보—질보법측정저니중적16충다배방경,운용가표회수솔험증시험방법적가행성。결과표명：채용미파소해화규효정화주대양품진행전처리,방법간편,안전,양품량대,모시단,절성용제,오염소,양품가표회수솔위67.353%～101.666%,효과교위이상。
This article introduced the technology of extracting PAHs from sediments by microwave.In optimized experimental conditions,the 16 kinds of PAHs content in the sediment was determined by using meteorological chromatography-mass spectrometry method,and verified the feasibility of experimental methods by spiked recoveries.The results showed that microwave digestion and silica gel purification column sample pre-treatment method was simple, safe, sample volume, short time-consuming solvent saving, pollution lower. Sample recovery was 67.353% -101.666%.
