海南师范大学学报:自然科学版
海南師範大學學報:自然科學版
해남사범대학학보:자연과학판
Journal of Hainan Normal University:Natural Science
2012年
3期
292-294,303
,共4页
张利%李响%何颖%王会玲%王恩举
張利%李響%何穎%王會玲%王恩舉
장리%리향%하영%왕회령%왕은거
微晶纤维素%β-环糊精%接枝率
微晶纖維素%β-環糊精%接枝率
미정섬유소%β-배호정%접지솔
Mierocrystalline cellulose%β-Cyclodextrin%Grafting ratio
在碱性条件性下,以环氧氯丙烷为联接剂将俨环糊精接枝到微晶纤维素表面.通过紫外分光光度法研究了该功能化纤维素对肉桂酸的包合吸附能力,每克纤维素可吸附18.375mg肉桂酸,产品中β-环糊精的质量分数高达14%.纤维素表面的β-环糊精保留了天然环糊精的包合特性,是一种优良的固相萃取剂.
在堿性條件性下,以環氧氯丙烷為聯接劑將儼環糊精接枝到微晶纖維素錶麵.通過紫外分光光度法研究瞭該功能化纖維素對肉桂痠的包閤吸附能力,每剋纖維素可吸附18.375mg肉桂痠,產品中β-環糊精的質量分數高達14%.纖維素錶麵的β-環糊精保留瞭天然環糊精的包閤特性,是一種優良的固相萃取劑.
재감성조건성하,이배양록병완위련접제장엄배호정접지도미정섬유소표면.통과자외분광광도법연구료해공능화섬유소대육계산적포합흡부능력,매극섬유소가흡부18.375mg육계산,산품중β-배호정적질량분수고체14%.섬유소표면적β-배호정보류료천연배호정적포합특성,시일충우량적고상췌취제.
Under alkaline condition,β-cyclodextrin (β-CD) was grafted onto microcrystalline cellulose powder by us- ing epiehlorohydrin as a chemical linking agent to afford a type of functionalized cellulose. The adsorption behavior of cinnamic acid on the funetionalized cellulose was determined by UV spectrophotometry, and the adsorption capability was 18.375mg-g-1. The mass fraction of β-CD in the product reached up to 14 percent. The β-CD supported on cellulose preserved the inclusion ability as natural β-CD.