CAJ | 학술논문

：为建立非水电位滴定法测定阿戈美拉汀工作对照品的含量，采用非水电位滴定法以氯仿一醋酐（6：1）为溶剂，用高氯酸滴定液（O．1mol/L）进行滴定．实验结果表明，非水电位滴定法的方法的相对标准偏差（RSD）为0．1％（n=9），平均回收率为99．8％，测定结果在统计学上无显著性差异．该方法简便快速，结果准确可靠．
：위건립비수전위적정법측정아과미랍정공작대조품적함량，채용비수전위적정법이록방일작항（6：1）위용제，용고록산적정액（O．1mol/L）진행적정．실험결과표명，비수전위적정법적방법적상대표준편차（RSD）위0．1％（n=9），평균회수솔위99．8％，측정결과재통계학상무현저성차이．해방법간편쾌속，결과준학가고．
To establish a non-aqueous potentiometry titration method for the content detenrrination of agome- latine working standard, trichloromethane and acetic anhydride(6: 1) were used as solvent for non-aqueous potentiomerry titration. 0.1 mol/L perchloric acid was used to titrate the content of agomelatine working standard. Results show that the conditions of non-aqueous potentiometry titration are the followings: the pre- cision RSD is 0.1% (n = 9), the average recovery is 99.8 %. It is concluded that the outcome obtained by non-aqueous potentimetry titration method has no statistical difference. This method is simple and fast with accurate and countable results.