CAJ | 학술논문

在醋酸钠体系中,以α-α联吡啶为活化剂,用镍催化过硫酸钾氧化二氯荧光素,建立了测量海产品中的痕量镍催化动力学荧光法的分析方法.实验相关系数R=0.993 23,线性范围为0.5～5μg/L,相对标准偏差为2.94%,检出限为3.7×10-6μg/L.用该方法测定文蛤汁中的镍含量,结果令人满意.
재작산납체계중,이α-α련필정위활화제,용얼최화과류산갑양화이록형광소,건립료측량해산품중적흔량얼최화동역학형광법적분석방법.실험상관계수R=0.993 23,선성범위위0.5～5μg/L,상대표준편차위2.94%,검출한위3.7×10-6μg/L.용해방법측정문합즙중적얼함량,결과령인만의.
A new catalytic kinetic fluorescence method for determination of trace nickel has been set up in NaAc system.This method is based on the catalytic oxidation of two chlorine fluoresceins by α-α dipyridyl as an activator.With correlation data R is 0.993 23,the linear range of determination is 0.5~5 μg/L for Ni,the detection limit is 3.7×10-6 μg/L.This method can be applied to the trace nickel in meretrix with satisfactory results.