广州大学学报:自然科学版
廣州大學學報:自然科學版
엄주대학학보:자연과학판
Journal og Guangzhou University:Natural Science Edition
2012年
4期
90-93
,共4页
催化发光%传感器%薄膜制备
催化髮光%傳感器%薄膜製備
최화발광%전감기%박막제비
cataluminescence%sensor%thin film preparing
本研究用溶胶-凝胶法制备MgO和In2O3纳米薄膜材料前躯体,用浸渍镀膜法制备纳米薄膜.讨论了MgO和In2O3薄膜在不同的胶体制备pH值、煅烧温度和镀膜层数下,对一些有机气体的催化发光信号强度的影响.通过实验数据分析得出,MgO纳米薄膜在胶体制备pH为8、镀膜层数为5层、煅烧温度为550℃的条件下对乙二醇甲醚等蒸气具有最佳的催化发光信号.In2O3纳米薄膜在胶体制备pH为5、镀膜层数为5层、煅烧温度为550℃的条件下,对乙酸等蒸气具有最佳的催化发光信号.
本研究用溶膠-凝膠法製備MgO和In2O3納米薄膜材料前軀體,用浸漬鍍膜法製備納米薄膜.討論瞭MgO和In2O3薄膜在不同的膠體製備pH值、煅燒溫度和鍍膜層數下,對一些有機氣體的催化髮光信號彊度的影響.通過實驗數據分析得齣,MgO納米薄膜在膠體製備pH為8、鍍膜層數為5層、煅燒溫度為550℃的條件下對乙二醇甲醚等蒸氣具有最佳的催化髮光信號.In2O3納米薄膜在膠體製備pH為5、鍍膜層數為5層、煅燒溫度為550℃的條件下,對乙痠等蒸氣具有最佳的催化髮光信號.
본연구용용효-응효법제비MgO화In2O3납미박막재료전구체,용침지도막법제비납미박막.토론료MgO화In2O3박막재불동적효체제비pH치、단소온도화도막층수하,대일사유궤기체적최화발광신호강도적영향.통과실험수거분석득출,MgO납미박막재효체제비pH위8、도막층수위5층、단소온도위550℃적조건하대을이순갑미등증기구유최가적최화발광신호.In2O3납미박막재효체제비pH위5、도막층수위5층、단소온도위550℃적조건하,대을산등증기구유최가적최화발광신호.
Nano-thin films precursors of MgO and In2O3 were synthesized by sol-gel method and thin films were prepared by dip coating method. The influence of eataluminescence (CTL) signals of some organic gases on MgO thin film and In:O3 thin film with the preparing condition of colloid solution pH, calcination temperature and film layers were discussed. From the experimental data analysis, we can conclude that for detecting ethylene glycol methyl ether vapor, MgO thin film has the optimum CTL signal, under the condition as follows: the colloid solution of pH = 8, calcinations temperature of 550 ℃, coating film of 5 layers. For detection of acetic acid vapor, In2O3thin film has the optimum CTL signal, under the condition as follows: the colloid solution of pH = 5, calcinations temperature of 550 ℃, coating film of 5 layers.