中国现代药物应用
中國現代藥物應用
중국현대약물응용
CHINESE JOURNAL OF MODERN DRUG APPLICATION
2014年
7期
5-6
,共2页
苦参炭%薄层色谱%展开剂
苦參炭%薄層色譜%展開劑
고삼탄%박층색보%전개제
Sophora carbon%TLC identification%Developing solvent
目的:研究苦参炭的薄层色谱鉴别。方法选用甲苯-丙酮-甲醇(8:3:1.5)为展开剂,浓氨水饱和,碘化铋钾试液为显色剂,以苦参碱、槐定碱、氧化苦参碱为对照品进行薄层鉴别。结果选用甲苯-丙酮-甲醇(8:3:1.5)为展开剂,碘化铋钾试液为显色剂进行薄层鉴别,色谱斑点清晰,能有效提供鉴别特征。结论方法可行,为建立完整、科学的苦参炭质量标准提供了参考依据。
目的:研究苦參炭的薄層色譜鑒彆。方法選用甲苯-丙酮-甲醇(8:3:1.5)為展開劑,濃氨水飽和,碘化鉍鉀試液為顯色劑,以苦參堿、槐定堿、氧化苦參堿為對照品進行薄層鑒彆。結果選用甲苯-丙酮-甲醇(8:3:1.5)為展開劑,碘化鉍鉀試液為顯色劑進行薄層鑒彆,色譜斑點清晰,能有效提供鑒彆特徵。結論方法可行,為建立完整、科學的苦參炭質量標準提供瞭參攷依據。
목적:연구고삼탄적박층색보감별。방법선용갑분-병동-갑순(8:3:1.5)위전개제,농안수포화,전화필갑시액위현색제,이고삼감、괴정감、양화고삼감위대조품진행박층감별。결과선용갑분-병동-갑순(8:3:1.5)위전개제,전화필갑시액위현색제진행박층감별,색보반점청석,능유효제공감별특정。결론방법가행,위건립완정、과학적고삼탄질량표준제공료삼고의거。
Objective To study identification of sophora carbon TLC. Methods Selecting toluene-pain-methanol (8:3:1.5) as developing agent,using saturation strong aqua,taking bismuth potassium iodide solution as the chromogenic agent, and setting matrine, huaialkali,bitter and alkali oxide TLC identification for reference substance. Results Selects the toluene-acetone-methanol (8:3:1. 5) as developing solvent, Bismuth potassium iodide solution for TLC identification as the chromogenic agent,the chromatographic spots were clear, and can effectively provide identification features. Conclusion The method is feasible, and can be a reference to establish a complete, scientific sophora charcoal for quality standards.