中医药信息
中醫藥信息
중의약신식
INFORMATION ON TRADITIONAL CHINESE MEDICINE
2014年
3期
92-94
,共3页
侯文慧%石晋丽%刘勇%刘倩佟%史淑宁%刘洁%李鹤
侯文慧%石晉麗%劉勇%劉倩佟%史淑寧%劉潔%李鶴
후문혜%석진려%류용%류천동%사숙저%류길%리학
蜘蛛香%缬草三酯类化合物%降解产物%11-ethoxyviburtinal%正交实验%提取工艺
蜘蛛香%纈草三酯類化閤物%降解產物%11-ethoxyviburtinal%正交實驗%提取工藝
지주향%힐초삼지류화합물%강해산물%11-ethoxyviburtinal%정교실험%제취공예
Valeriana jatamansi Jones%Valepotriates%Degraded product%11-ethoxyviburtinal%Orthogonal ex-periment%Extraction technology
目的:以11-ethoxyviburtinal的含量为指标,优选蜘蛛香的提取工艺。方法:分别以药材的粉碎程度、提取时间、提取次数和溶剂倍数为考察因素,以化合物11-ethoxyviburtinal 为指标性成分,采用正交实验法,优选蜘蛛香的提取工艺。结果:蜘蛛香的最佳提取工艺为A3 B2 C1 D3,即:将蜘蛛香粉碎成细粉,加10倍量35%乙醇,加热回流提取2次,每次1 h。结论:以10倍量35%乙醇加热回流提取蜘蛛香的方法稳定可行,可为蜘蛛香的后期开发提供实验依据。
目的:以11-ethoxyviburtinal的含量為指標,優選蜘蛛香的提取工藝。方法:分彆以藥材的粉碎程度、提取時間、提取次數和溶劑倍數為攷察因素,以化閤物11-ethoxyviburtinal 為指標性成分,採用正交實驗法,優選蜘蛛香的提取工藝。結果:蜘蛛香的最佳提取工藝為A3 B2 C1 D3,即:將蜘蛛香粉碎成細粉,加10倍量35%乙醇,加熱迴流提取2次,每次1 h。結論:以10倍量35%乙醇加熱迴流提取蜘蛛香的方法穩定可行,可為蜘蛛香的後期開髮提供實驗依據。
목적:이11-ethoxyviburtinal적함량위지표,우선지주향적제취공예。방법:분별이약재적분쇄정도、제취시간、제취차수화용제배수위고찰인소,이화합물11-ethoxyviburtinal 위지표성성분,채용정교실험법,우선지주향적제취공예。결과:지주향적최가제취공예위A3 B2 C1 D3,즉:장지주향분쇄성세분,가10배량35%을순,가열회류제취2차,매차1 h。결론:이10배량35%을순가열회류제취지주향적방법은정가행,가위지주향적후기개발제공실험의거。
Objective:Take compound 11-ethoxyviburtinal as an index component , and optimize the extraction technology of 11 -ethoxyviburtinal from Valeriana jatamansi Jones . Methods: Take compound 11 -ethoxyviburtinal as an index component , and degree of pulverization , extraction time , times of extraction and solvent ratio were considered ,and the extraction technology of Valeriana jatamansi Jones was optimized by Or-thogonal Design .Results:Through orthogonal experiment analysis , the optimum extraction technology of Vale-riana jatamansi Jones was A 3 B2 C1 D3 , making into fine powder , with 10 times amount of 35%alcohol adding , Valeriana jatamansi Jones was refluxed and extracted for two times , each time for one hour .Conclusion:This method is stable and feasible , which can provide experimental basis for the further development of Valeriana jatamansi Jones .