化学分析计量
化學分析計量
화학분석계량
CHEMICAL ANALYSIS AND METERAGE
2013年
6期
88-90
,共3页
紫外光%臭氧%总磷%离子色谱法
紫外光%臭氧%總燐%離子色譜法
자외광%취양%총린%리자색보법
ultraviolet light%ozone%total phosphorus%ion chromatography
采用紫外光与臭氧结合消解水样,用离子色谱法测定水质总磷含量,色谱峰高与磷酸盐质量浓度在0~20 mg/L范围内线性关系良好,检出限和测定下限分别0.008 mg/L和0.03 mg/L。此方法无需添加化学试剂,避免了标准分析方法中各种因素的影响,操作简单快速、省时,测定水质总磷的相对标准偏差为0.07%(n=5)。对实际样品进行分析,总磷的加标回收率为94.5%~105.5%,表明该方法测定结果可靠,具有一定的应用价值。
採用紫外光與臭氧結閤消解水樣,用離子色譜法測定水質總燐含量,色譜峰高與燐痠鹽質量濃度在0~20 mg/L範圍內線性關繫良好,檢齣限和測定下限分彆0.008 mg/L和0.03 mg/L。此方法無需添加化學試劑,避免瞭標準分析方法中各種因素的影響,操作簡單快速、省時,測定水質總燐的相對標準偏差為0.07%(n=5)。對實際樣品進行分析,總燐的加標迴收率為94.5%~105.5%,錶明該方法測定結果可靠,具有一定的應用價值。
채용자외광여취양결합소해수양,용리자색보법측정수질총린함량,색보봉고여린산염질량농도재0~20 mg/L범위내선성관계량호,검출한화측정하한분별0.008 mg/L화0.03 mg/L。차방법무수첨가화학시제,피면료표준분석방법중각충인소적영향,조작간단쾌속、성시,측정수질총린적상대표준편차위0.07%(n=5)。대실제양품진행분석,총린적가표회수솔위94.5%~105.5%,표명해방법측정결과가고,구유일정적응용개치。
Digested by ultraviolet ray combined with ozone, total phosphorus content in water was determined by ion chromatography. There was good linearity between chromatographic peak height and the concentration of phosphate in the range of 0-20 mg/L. The detection limit and low limit were 0.008 mg/L and 0.03 mg/L, respectively. Without add-ing chemical reagents, this method avoid the influence of various factors in the standard analysis method. The operation is simple and quick, save time. The RSD of determination results was 0.07%(n=5). For real samples analysis, the recovery rate was 94.5%-105.5%, which showed that the method was reliable and had application value.