资源调查与环境
資源調查與環境
자원조사여배경
RESOURCES SURVEY & ENVIRONMENT
2012年
1期
40-45
,共6页
宋如晟%钟鸣%陈婉露%余红梅
宋如晟%鐘鳴%陳婉露%餘紅梅
송여성%종명%진완로%여홍매
沙坪沟钼矿%样品制备%分析质量监控
沙坪溝鉬礦%樣品製備%分析質量鑑控
사평구목광%양품제비%분석질량감공
Shapinggou molybdenum deposit%sampling preparation%quality supervisory control
通过对安徽省沙坪沟钼矿床矿石物质成分及结构、构造的分析,发现矿石中辉钼矿常呈细小鳞片状、浸染状分布于细脉中。针对岩芯易沿含矿裂纹破裂造成鳞片状辉钼矿丢失,本矿区全部采用金刚石刀具切割分取岩芯。制样过程试验中将样品无缩分粗碎、中碎至Ф〈-1.0mm,进行了K值试验,取0.5。缩分后密封棒磨6小时(充分混匀、磨碎)至-200目。分析了该矿区伴生元素不干扰测定的情况,不加Fe:O。载体,刚玉坩埚-Na2O2熔矿,降低空白值,严格质量监控,采用硫氰酸盐分光光度法测定钼量,获得的结果稳定可靠。本试验成果可为从事同类型大型钼矿的分析测试和质量监控提供参考。
通過對安徽省沙坪溝鉬礦床礦石物質成分及結構、構造的分析,髮現礦石中輝鉬礦常呈細小鱗片狀、浸染狀分佈于細脈中。針對巖芯易沿含礦裂紋破裂造成鱗片狀輝鉬礦丟失,本礦區全部採用金剛石刀具切割分取巖芯。製樣過程試驗中將樣品無縮分粗碎、中碎至Ф〈-1.0mm,進行瞭K值試驗,取0.5。縮分後密封棒磨6小時(充分混勻、磨碎)至-200目。分析瞭該礦區伴生元素不榦擾測定的情況,不加Fe:O。載體,剛玉坩堝-Na2O2鎔礦,降低空白值,嚴格質量鑑控,採用硫氰痠鹽分光光度法測定鉬量,穫得的結果穩定可靠。本試驗成果可為從事同類型大型鉬礦的分析測試和質量鑑控提供參攷。
통과대안휘성사평구목광상광석물질성분급결구、구조적분석,발현광석중휘목광상정세소린편상、침염상분포우세맥중。침대암심역연함광렬문파렬조성린편상휘목광주실,본광구전부채용금강석도구절할분취암심。제양과정시험중장양품무축분조쇄、중쇄지Ф〈-1.0mm,진행료K치시험,취0.5。축분후밀봉봉마6소시(충분혼균、마쇄)지-200목。분석료해광구반생원소불간우측정적정황,불가Fe:O。재체,강옥감과-Na2O2용광,강저공백치,엄격질량감공,채용류청산염분광광도법측정목량,획득적결과은정가고。본시험성과가위종사동류형대형목광적분석측시화질량감공제공삼고。
By studying on the material composition,texture and structure of ores of Shapinggou molybdenum deposit, Anhui province, it is found that molybdenites in the ores often present as small scale like and dis seminated minerals distributed in veinlets. To counter the situation that the rock cores are easily disrupted along the orebearing cracks, inducing the scalelike molybdenites to be losted, the diamond cutting tools were used to cut the cores in the present experiment. In the testing of sampling preparation, the sample was processed by nonreduction primary crushing, secondary crushing to Ф〈-1.0 mm and testing of K value for sample reduction (adopted K=0.5). Then, the reduced sample was sealed up and crushed to-200 meshes by rod milling for 6 hours (fully mixing and grinding). As the associated elements in the ores show no interference with the determination of Mo-content, in the conditions of no addition of Fe203 carrier, melting ore with corundum crucible Na202,reducing blank values and strict quality supervisory control, the method of thiocyanate spectrophotometric analysis for determination of Mocontent gave stable and reliable results, which can provide a reference in the testing and quality supervisory control for the same type of largescale molybdenum deposits.