福建分析测试
福建分析測試
복건분석측시
FUJIAN ANALYSIS & TESTING
2012年
2期
45-47
,共3页
火焰原子吸收光谱法%三硅酸镁%镁%含量测定
火燄原子吸收光譜法%三硅痠鎂%鎂%含量測定
화염원자흡수광보법%삼규산미%미%함량측정
FAAS%compound Bbndazol and hdrochlorothiazide capsules%magnesium oxide%determination
目的:建立三硅酸镁中镁的含量测定方法。方法:样品微波消解处理后,火焰原子吸收光谱法测定样品中镁的含量。结果:镁在0.05-0.4mg/L范围内线性关系良好,相关系数为0.9995;回收率在98.4%-102.9%,RSD为1.5%。结论:该方法简单、快速、准确;能很好地用于三硅酸镁中镁的质量控制。
目的:建立三硅痠鎂中鎂的含量測定方法。方法:樣品微波消解處理後,火燄原子吸收光譜法測定樣品中鎂的含量。結果:鎂在0.05-0.4mg/L範圍內線性關繫良好,相關繫數為0.9995;迴收率在98.4%-102.9%,RSD為1.5%。結論:該方法簡單、快速、準確;能很好地用于三硅痠鎂中鎂的質量控製。
목적:건립삼규산미중미적함량측정방법。방법:양품미파소해처리후,화염원자흡수광보법측정양품중미적함량。결과:미재0.05-0.4mg/L범위내선성관계량호,상관계수위0.9995;회수솔재98.4%-102.9%,RSD위1.5%。결론:해방법간단、쾌속、준학;능흔호지용우삼규산미중미적질량공제。
To establish a method to determine magnesium in magnesium trisilicate. Method: The sample was handled by Microwave Digestion System, the content of magnesium in the samples was determinated by FAAS. Result: The good linear relation was determined as 0.05-0.4 mg.L-1 in magnesium by FAAS with a regression coeffcient of 0.9995. The average recovery rate was 98.4%-102.9% ;The relative standard deviation was 1.5%. Conclusion:The method was simple, rapid and accurate, and can be used for quality control of magnesium in magnesium trisilicate.