CAJ | 학술논문

原子荧光光谱法测定地下水锡试验中,选择最佳的硼氢化钾溶液和硫脲-抗坏血酸溶液浓度,反应体系中加入浓度为20 g/L硼氢化钾溶液,100 mL试样溶液中加入10 mL硫脲-抗坏血酸溶液作为还原剂,方法检出限为0.02μg/L,测量精密度为0.33%～1.24%,加标回收效率为100%～102%。
원자형광광보법측정지하수석시험중,선택최가적붕경화갑용액화류뇨-항배혈산용액농도,반응체계중가입농도위20 g/L붕경화갑용액,100 mL시양용액중가입10 mL류뇨-항배혈산용액작위환원제,방법검출한위0.02μg/L,측량정밀도위0.33%～1.24%,가표회수효솔위100%～102%。
Determination of tin in water test was studied with atomic fluorescence spectrometry,choosing the best potassium borohydride solution and thiourea L-ascorbic acid solution concentration,the reaction system with the concentration of 20 g/L potassium borohydride solution,sample solution of thiourea in 100 mL joined the 10 mL-ascorbic acid as the reducing agent,the detection limit was 0.02 g/L,measuring precision degree was 0.33% to 1.24%,and the recovery rate was 100%~102%.