农药科学与管理
農藥科學與管理
농약과학여관리
PESTICIDE SCIENCE AND ADMINISTRATION
2012年
3期
19-22
,共4页
刘振邦%董立峰%王智%张保华
劉振邦%董立峰%王智%張保華
류진방%동립봉%왕지%장보화
联苯菊酯%水乳剂%配方筛选%正交优化
聯苯菊酯%水乳劑%配方篩選%正交優化
련분국지%수유제%배방사선%정교우화
bifenthrin%emulsion in water%formulation selection%orthogonal experiment
本研究通过正交优化得到联苯菊酯10%水乳剂的最佳配方:联苯菊酯原药10%,二甲苯20%,农乳602#3.5%,Tween-20 2.5%,农乳500#2%,乙二醇4%,有机硅消泡剂0.2%,去离子水补足至100%。最佳生产工艺为:使用高速剪切机,剪切转速6 000r/min,剪切时间4min。该水乳剂pH值5.7~6.5,稀释100倍于(30±2)℃恒温水浴24h未出现浮油、沉油、沉淀,经(54±2)℃热贮14d,分解率〈2%,制剂表面张力低,倾倒性佳。
本研究通過正交優化得到聯苯菊酯10%水乳劑的最佳配方:聯苯菊酯原藥10%,二甲苯20%,農乳602#3.5%,Tween-20 2.5%,農乳500#2%,乙二醇4%,有機硅消泡劑0.2%,去離子水補足至100%。最佳生產工藝為:使用高速剪切機,剪切轉速6 000r/min,剪切時間4min。該水乳劑pH值5.7~6.5,稀釋100倍于(30±2)℃恆溫水浴24h未齣現浮油、沉油、沉澱,經(54±2)℃熱貯14d,分解率〈2%,製劑錶麵張力低,傾倒性佳。
본연구통과정교우화득도련분국지10%수유제적최가배방:련분국지원약10%,이갑분20%,농유602#3.5%,Tween-20 2.5%,농유500#2%,을이순4%,유궤규소포제0.2%,거리자수보족지100%。최가생산공예위:사용고속전절궤,전절전속6 000r/min,전절시간4min。해수유제pH치5.7~6.5,희석100배우(30±2)℃항온수욕24h미출현부유、침유、침정,경(54±2)℃열저14d,분해솔〈2%,제제표면장력저,경도성가。
The optimum formulation of 10% bifenthrin emulsion in water(EW)was developed by the screening of the solvent and surfactant through the orthogonal experiment.The optimum solvent was 18% dimethylbenzene,the optimum surfactants of 602# and Tween-20 and 500# were 3% and 2.5% and 2%,the ethanediol was 4%,the organic silicon defoamer was 0.2%,the other component was deionized water.The best productive technology of 10% bifenthrin EW was that the shearing speed was 6 000 r/min,and the shearing time fixed on 4 mins.The pH was 5.7~6.5,there were not oil slick,precipitation,the stability of the bifenthrin EW was up to grade.The formulation had been stored at the temperature(54±2)℃for14 days with the resolution ratio 1.5%,its surface tension was low enough,and good pourability it had.