功能材料
功能材料
공능재료
JOURNAL OF FUNCTIONAL MATERIALS
2014年
7期
7022-7026
,共5页
预变形量%形状回复率%Fe-Mn-Si-Cr-Ni-C合金%Cr23 C6 颗粒
預變形量%形狀迴複率%Fe-Mn-Si-Cr-Ni-C閤金%Cr23 C6 顆粒
예변형량%형상회복솔%Fe-Mn-Si-Cr-Ni-C합금%Cr23 C6 과립
amount of pre-deformation%shape recovery ratio%Fe-Mn-Si-Cr-Ni-C alloy%Cr23 C6 particle
为了进一步提高 Fe13Mn6Si13Cr4Ni0.1C合金的形状记忆效应,研究了不同预变形量对1073 K时效合金的组织及形状记忆效应的影响.研究结果表明,10%预变形后再时效的合金,形状回复率在时效300 min 时达到(86.1±1.0)%,比固溶态32%提高了169%;5%预变形后再时效的合金,在180 min 时达到最大值(82.9±1.0)%,比固溶态提高了159%,随后形状回复率随时效时间延长略有下降;直接时效合金(无预变形量),在180 min 时达到最大值(46.3±1.0)%,比固溶态提高了44.7%,随后形状回复率也随时效时间延长略有下降.经 SEM 和 XRD 分析,10%预变形后再时效合金所析出的定向 Cr23 C6颗粒最多,也最细小,这是此合金比5%预变形后再时效合金以及直接时效合金形状回复率提高幅度更大的原因.
為瞭進一步提高 Fe13Mn6Si13Cr4Ni0.1C閤金的形狀記憶效應,研究瞭不同預變形量對1073 K時效閤金的組織及形狀記憶效應的影響.研究結果錶明,10%預變形後再時效的閤金,形狀迴複率在時效300 min 時達到(86.1±1.0)%,比固溶態32%提高瞭169%;5%預變形後再時效的閤金,在180 min 時達到最大值(82.9±1.0)%,比固溶態提高瞭159%,隨後形狀迴複率隨時效時間延長略有下降;直接時效閤金(無預變形量),在180 min 時達到最大值(46.3±1.0)%,比固溶態提高瞭44.7%,隨後形狀迴複率也隨時效時間延長略有下降.經 SEM 和 XRD 分析,10%預變形後再時效閤金所析齣的定嚮 Cr23 C6顆粒最多,也最細小,這是此閤金比5%預變形後再時效閤金以及直接時效閤金形狀迴複率提高幅度更大的原因.
위료진일보제고 Fe13Mn6Si13Cr4Ni0.1C합금적형상기억효응,연구료불동예변형량대1073 K시효합금적조직급형상기억효응적영향.연구결과표명,10%예변형후재시효적합금,형상회복솔재시효300 min 시체도(86.1±1.0)%,비고용태32%제고료169%;5%예변형후재시효적합금,재180 min 시체도최대치(82.9±1.0)%,비고용태제고료159%,수후형상회복솔수시효시간연장략유하강;직접시효합금(무예변형량),재180 min 시체도최대치(46.3±1.0)%,비고용태제고료44.7%,수후형상회복솔야수시효시간연장략유하강.경 SEM 화 XRD 분석,10%예변형후재시효합금소석출적정향 Cr23 C6과립최다,야최세소,저시차합금비5%예변형후재시효합금이급직접시효합금형상회복솔제고폭도경대적원인.
To further improve shape memory effect in a Fe13Mn6Si13Cr4Ni0.1C alloy,the effect of different amount of pre-deformation on microstructure and shape memory effect in alloys aged at 1 073 K was studied. The results showed that the shape recovery ration in alloys aged after 10% pre-deformation can reach (86.1±1. 0)% at 300 min,increased by 1 69% compared to 32% in a water-quenching alloy.And the shape recovery ra-tion in aged alloys following 5% pre-deformation rises up to the maximum value (82.9±1.0)% at 180 min,in-crease by 159% compared with 32%,but it slightly decreases with ageing time over 180 min.The shape recov-ery ration for directly aged alloys without pre-deformation reaches the peak value (46.3 ± 1.0)% at 180 min, higher 44.7% than 32%,but it gradually falls down over 180 min.By SEM and XRD analysis it was found that aligned Cr23 C6 particles precipitated from alloys aged after 10% pre-deformation are the most,the smallest a-mong the above three alloys.It was just the reason that makes more improvement in shape memory ration for aged alloys following 10% pre-deformation than that for alloys aged after 5% pre-deformation and directly aged alloys.