CAJ | 학술논문

采用顶空固相微萃取-气相色谱质谱联用（HS-SPME-GC-MS）技术分析比较鲜艾叶与干艾叶的挥发性成分。考察了不同萃取头和萃取温度对艾叶挥发性成分的萃取效果,以选用65μm PDMS/DVB SPME萃取头和60℃水浴加热时萃取效果最好;采用峰面积归一化法测定各成分的质量分数,共鉴定出58种挥发性成分,主要为烯烃类、芳香类和醇类物质,占总峰面积90%以上。鲜艾叶与干艾叶均含有莰烯、1-辛烯-3-醇、α-水芹烯、邻聚伞花素、桉油精、石竹烯等,此外又各自具有特有成分,表明艾叶在干制后其挥发性成分发生变化。
채용정공고상미췌취-기상색보질보련용（HS-SPME-GC-MS）기술분석비교선애협여간애협적휘발성성분。고찰료불동췌취두화췌취온도대애협휘발성성분적췌취효과,이선용65μm PDMS/DVB SPME췌취두화60℃수욕가열시췌취효과최호;채용봉면적귀일화법측정각성분적질량분수,공감정출58충휘발성성분,주요위희경류、방향류화순류물질,점총봉면적90%이상。선애협여간애협균함유감희、1-신희-3-순、α-수근희、린취산화소、안유정、석죽희등,차외우각자구유특유성분,표명애협재간제후기휘발성성분발생변화。
We analyzed volatile components in fresh and dried leaves of Artemisia argyi Levl.et Vant.with headspace solid phase microextraction（SPME） and GC-MS.We also investigated the impacts of different SPME fibers and extraction temperature on the extracts.Results demonstrate that 65 μm PDMS/DVB fibre and temperature of 60 ℃ exhibit good extraction effect.We employed peak area normalization method to determine the volatile components.Fifty-eight compounds are identified in the fresh and dried leaves of Artemisia argyi,which include alkanes,alkenes and alcohols,and whose area exceeds 90% of the total peak area.Results also show that fresh and dried leaves of Artemisia argyi not only contain identical volatile compounds such as Camphene,1-Octen-3-ol,alpha-Phellandrene,Benzene,1-methyl-2-（1-methylethyl）-Eucalyptol and Caryophyllene,but also contain their own unique volatile compounds.This shows that their volatile components change after dryness.