韶关学院学报
韶關學院學報
소관학원학보
JOURNAL OF SHAOGUAN UNIVERSITY(SOCIAL SCIENCE)
2012年
8期
56-58
,共3页
发光材料%红色长余辉%燃烧法%硫氧化钇
髮光材料%紅色長餘輝%燃燒法%硫氧化釔
발광재료%홍색장여휘%연소법%류양화을
Phosphor%red long afterglow%combustion synthesis%Y202S
用燃烧法成功合成了纳米Y2O2S:Eu3+,Mg2+,Ti4+红色长余辉发光材料,采用X射线粉末衍射仪(XRD)、扫描电镜(SEM)、荧光光谱仪(PL)对样品进行了物相组成、显微形貌、激发发射光谱等进行了表征.样品的主要组成为Y2O2S;呈厚度为40~70 nm,直径为100~200 nm的纳米片;在626 nm和617 nm处有强烈的红色发射.与固相法比较,激发光谱略有蓝移.
用燃燒法成功閤成瞭納米Y2O2S:Eu3+,Mg2+,Ti4+紅色長餘輝髮光材料,採用X射線粉末衍射儀(XRD)、掃描電鏡(SEM)、熒光光譜儀(PL)對樣品進行瞭物相組成、顯微形貌、激髮髮射光譜等進行瞭錶徵.樣品的主要組成為Y2O2S;呈厚度為40~70 nm,直徑為100~200 nm的納米片;在626 nm和617 nm處有彊烈的紅色髮射.與固相法比較,激髮光譜略有藍移.
용연소법성공합성료납미Y2O2S:Eu3+,Mg2+,Ti4+홍색장여휘발광재료,채용X사선분말연사의(XRD)、소묘전경(SEM)、형광광보의(PL)대양품진행료물상조성、현미형모、격발발사광보등진행료표정.양품적주요조성위Y2O2S;정후도위40~70 nm,직경위100~200 nm적납미편;재626 nm화617 nm처유강렬적홍색발사.여고상법비교,격발광보략유람이.
NanocrystallineY202S: Eu3+, Mg2+, Ti4+ red long afterglow phosphor was successfully fabricated by combustion synthesis. The phase composition, morphology and luminescence properties were investigated by X- ray diffraction (XRD), scanning electron microscopy (SEM) and photolumineseence (PL) spectra. The morphology of the sample was circular nanosheets with thickness in range of 40-70 nm and diameter in range of 100~200 nm. The Y202S: Eu3+, Mg2+, Ti4+exhibited strong red emission at 626 nm and 617 nm. Compared Y202S: Eu3+, Mg2+, Ti4+ material, the excitation peak of nanocrystalline phosphor showed apparent excitation spectrum. with the bulk blue-shift in