广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2012年
17期
128-129
,共2页
郑阿龙%张存社%沈寒晰%郭鹏涛
鄭阿龍%張存社%瀋寒晰%郭鵬濤
정아룡%장존사%침한석%곽붕도
二甲基亚砜%间歇精馏%不稳定因素%解决措施
二甲基亞砜%間歇精餾%不穩定因素%解決措施
이갑기아풍%간헐정류%불은정인소%해결조시
DMSO%batch distillation%unstable factors%solutions
对工业间歇精馏生产二甲基亚砜遇到的系统持液及蒸汽压不稳定等工艺问题,进行了分析研究,在原有的工艺设备上,采用"大回流压塔,小回流采出"的操作措施,有效地解决了二甲基亚砜生产中遇到的上述工艺问题。实验结果表明:缩短产品合格时间,提高产品品质,增加单批产品数量,取得了良好的经济效益。
對工業間歇精餾生產二甲基亞砜遇到的繫統持液及蒸汽壓不穩定等工藝問題,進行瞭分析研究,在原有的工藝設備上,採用"大迴流壓塔,小迴流採齣"的操作措施,有效地解決瞭二甲基亞砜生產中遇到的上述工藝問題。實驗結果錶明:縮短產品閤格時間,提高產品品質,增加單批產品數量,取得瞭良好的經濟效益。
대공업간헐정류생산이갑기아풍우도적계통지액급증기압불은정등공예문제,진행료분석연구,재원유적공예설비상,채용"대회류압탑,소회류채출"적조작조시,유효지해결료이갑기아풍생산중우도적상술공예문제。실험결과표명:축단산품합격시간,제고산품품질,증가단비산품수량,취득료량호적경제효익。
The liquid holdup and the unstable vapor pressure were studied in the process of batch distillation DMSO production and in the original process equipment. A method using large back pressure tower and refluxthe recovery operation to effectively solve the problems was presented. The experimental results showed that through shortening the time of qualified products, improving product quality, and increasing of a single batch number of products, good economic benefits can be achieved.