广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2012年
17期
48-50
,共3页
徐小娜%蒋军辉%徐吉银%杨慧仙
徐小娜%蔣軍輝%徐吉銀%楊慧仙
서소나%장군휘%서길은%양혜선
枳实%超微粉碎%橙皮苷%柚皮苷
枳實%超微粉碎%橙皮苷%柚皮苷
지실%초미분쇄%등피감%유피감
Fructus Aurantii Immaturus%ultra - fine pulverization%hesperidin%naringin
探讨了超微粉碎对枳实药材中有效成分溶出率的影响。以0.05%磷酸水-甲醇-乙腈为流动相,采用高效液相色谱法（high performance liquid chromatography,HPLC）测定枳实超微粉与药材60目细粉中橙皮苷、柚皮苷和芸香柚皮苷的溶出率。结果表明,枳实超微粉中的橙皮苷、柚皮苷和芸香柚皮苷的溶出率明显高于其60目细粉中三者的溶出率,超微粉碎可增强枳实药材有效成分的溶出。
探討瞭超微粉碎對枳實藥材中有效成分溶齣率的影響。以0.05%燐痠水-甲醇-乙腈為流動相,採用高效液相色譜法（high performance liquid chromatography,HPLC）測定枳實超微粉與藥材60目細粉中橙皮苷、柚皮苷和蕓香柚皮苷的溶齣率。結果錶明,枳實超微粉中的橙皮苷、柚皮苷和蕓香柚皮苷的溶齣率明顯高于其60目細粉中三者的溶齣率,超微粉碎可增彊枳實藥材有效成分的溶齣。
탐토료초미분쇄대지실약재중유효성분용출솔적영향。이0.05%린산수-갑순-을정위류동상,채용고효액상색보법（high performance liquid chromatography,HPLC）측정지실초미분여약재60목세분중등피감、유피감화예향유피감적용출솔。결과표명,지실초미분중적등피감、유피감화예향유피감적용출솔명현고우기60목세분중삼자적용출솔,초미분쇄가증강지실약재유효성분적용출。
The effects of ultra - fine powder technique on dissolution rates of the flavonoids in Frutus Aurantii lmmaturus （FAI） were explored. Using 0. 05% H3PO4 water solution -CH3OH -CH3CN as mobile phase, high performance liquid chromatography was employed to determine the concentration of hesperidin, naringin and narirutin in common powdered and ultra - fine powdered FAI. The results were that the dissolution rates of hesperidin, naringin and narirutin in ultra - fine powdered FAI were higher than those of the general powder, and ultra - fine powder technique promoted the dissolution rates of effective constituents of herb medicine.
