陕西科技大学学报(自然科学版)
陝西科技大學學報(自然科學版)
협서과기대학학보(자연과학판)
JOURNAL OF SHAANXI UNIVERSITY OF SCIENCE & TECHNOLOGY
2014年
1期
119-122,147
,共5页
贯叶连翘%总黄酮%金丝桃素%超声提取
貫葉連翹%總黃酮%金絲桃素%超聲提取
관협련교%총황동%금사도소%초성제취
hypericum perforatum%flavonoids%hypericin%ultrasonic extraction
研究了从贯叶连翘中同时提取总黄酮和金丝桃素的最佳工艺条件,探讨了采用超声波辅助乙醇提取的方法来考查乙醇浓度、料液比、提取温度、提取时间、提取次数等因素对总黄酮和金丝桃素得率的影响,并结合正交试验确定最佳工艺.实验结果表明,最佳工艺参数为乙醇浓度70%、料液比1∶25、提取温度50℃、提取时间60 min、提取2次,总黄酮和金丝桃素的得率分别为7.02%和0.178%,采用此工艺提取快速、简便,为贯叶连翘资源的开发利用奠定了基础.
研究瞭從貫葉連翹中同時提取總黃酮和金絲桃素的最佳工藝條件,探討瞭採用超聲波輔助乙醇提取的方法來攷查乙醇濃度、料液比、提取溫度、提取時間、提取次數等因素對總黃酮和金絲桃素得率的影響,併結閤正交試驗確定最佳工藝.實驗結果錶明,最佳工藝參數為乙醇濃度70%、料液比1∶25、提取溫度50℃、提取時間60 min、提取2次,總黃酮和金絲桃素的得率分彆為7.02%和0.178%,採用此工藝提取快速、簡便,為貫葉連翹資源的開髮利用奠定瞭基礎.
연구료종관협련교중동시제취총황동화금사도소적최가공예조건,탐토료채용초성파보조을순제취적방법래고사을순농도、료액비、제취온도、제취시간、제취차수등인소대총황동화금사도소득솔적영향,병결합정교시험학정최가공예.실험결과표명,최가공예삼수위을순농도70%、료액비1∶25、제취온도50℃、제취시간60 min、제취2차,총황동화금사도소적득솔분별위7.02%화0.178%,채용차공예제취쾌속、간편,위관협련교자원적개발이용전정료기출.
The article researched the best process conditions on simultaneous extraction of to-tal flavonoids and hypericin from hypericum perforatum .,and explored the method of etha-nol ultrasonic assisted extraction to study the influences of ethanol concentration ,solid-liquid ratio ,extraction temperature ,extraction time ,extraction times on the yield of total fla-vonoids and hypericin .Then the extraction process was optimized by the orthogonal experi-ments .The result of the experiment shows that the optimum process conditions for ethanol ultrasonic assisted extraction technology of the total flavonoids and hypericin from hyperi-cum perforatum are ethanol concentration of 70% ,solid-liquid ratio of 1∶25 ,ultrasonic ex-traction temperature 50 ℃ ,extraction time 60 min ,extracted 2 times and the yield of hyperi-cin and flavonoids are 70 .18 mg/g and 0 .178% respectively ,the optimized technology is quick and simple and can be used for theoretical basic .