酿酒
釀酒
양주
LIQUOR MAKING
2013年
5期
76-78,79
,共4页
GC-MS%塑化剂%迁移量
GC-MS%塑化劑%遷移量
GC-MS%소화제%천이량
GC-MS%plasticizer%migration
目的：建立气相色谱-质谱联用（GC-MS）法测定蒸馏白酒中塑化剂浓度。方法：直接向白酒样品中加入内标物，运用GC-MS技术，采用选择离子质谱扫描（SIM）方式进行样品测定。结果：五种塑化剂的检测限在0.002-0.006mg/L之间，定量限在0.006-0.015mg/L之间，RSD均小于10%。结论：该研究方法具有快速简便、灵敏准确等特点，适用于蒸馏白酒中塑化剂浓度的测定。
目的：建立氣相色譜-質譜聯用（GC-MS）法測定蒸餾白酒中塑化劑濃度。方法：直接嚮白酒樣品中加入內標物，運用GC-MS技術，採用選擇離子質譜掃描（SIM）方式進行樣品測定。結果：五種塑化劑的檢測限在0.002-0.006mg/L之間，定量限在0.006-0.015mg/L之間，RSD均小于10%。結論：該研究方法具有快速簡便、靈敏準確等特點，適用于蒸餾白酒中塑化劑濃度的測定。
목적：건립기상색보-질보련용（GC-MS）법측정증류백주중소화제농도。방법：직접향백주양품중가입내표물，운용GC-MS기술，채용선택리자질보소묘（SIM）방식진행양품측정。결과：오충소화제적검측한재0.002-0.006mg/L지간，정량한재0.006-0.015mg/L지간，RSD균소우10%。결론：해연구방법구유쾌속간편、령민준학등특점，괄용우증류백주중소화제농도적측정。
Objective To establish the method to detect the plasticizer in distilled liquor by GC-MS. Method Directly added the internal standard to the liquor sample, using GC-MS techniques, the select monitoring mode was adopted in the MS determination. Result the detection limit of five plasticizing was between 0.002-0.006mg/L, the quantitative limit was between 0.006-0.015mg/L. The relative standard deviations were less than 10%. Conclusion The method is simple, rapid, sensitive and accurate, and it is suitable for analysis the plasticizer in distilled liquor.
