巢湖学院学报
巢湖學院學報
소호학원학보
CHAOHU TEACHERS COLLEGE JOURNAL
2013年
6期
44-47
,共4页
明胶%葡萄糖%银纳米粒子%绿色化学
明膠%葡萄糖%銀納米粒子%綠色化學
명효%포도당%은납미입자%록색화학
gelatin%D-glucose%silver nanoparticles%green chemistry
本文以明胶作为稳定剂,葡萄糖为还原剂,硝酸银(AgNO3)为前驱体,通过一条绿色途径合成了银纳米粒子。利用紫外-可见分光光度(UV-vis)、透射电子显微镜(TEM)、及X-射线衍射(XRD)对银纳米粒子的形貌、粒度及其分布进行了性能表征。结果表明:银纳米粒子颗粒呈球形,粒度均匀,单分散性较好。该合成方法实验条件简单、原料易得、反应温和且对环境无污染,因此在探索绿色纳米合成技术上具有很重要的借鉴意义和广阔的应用前景。
本文以明膠作為穩定劑,葡萄糖為還原劑,硝痠銀(AgNO3)為前驅體,通過一條綠色途徑閤成瞭銀納米粒子。利用紫外-可見分光光度(UV-vis)、透射電子顯微鏡(TEM)、及X-射線衍射(XRD)對銀納米粒子的形貌、粒度及其分佈進行瞭性能錶徵。結果錶明:銀納米粒子顆粒呈毬形,粒度均勻,單分散性較好。該閤成方法實驗條件簡單、原料易得、反應溫和且對環境無汙染,因此在探索綠色納米閤成技術上具有很重要的藉鑒意義和廣闊的應用前景。
본문이명효작위은정제,포도당위환원제,초산은(AgNO3)위전구체,통과일조록색도경합성료은납미입자。이용자외-가견분광광도(UV-vis)、투사전자현미경(TEM)、급X-사선연사(XRD)대은납미입자적형모、립도급기분포진행료성능표정。결과표명:은납미입자과립정구형,립도균균,단분산성교호。해합성방법실험조건간단、원료역득、반응온화차대배경무오염,인차재탐색록색납미합성기술상구유흔중요적차감의의화엄활적응용전경。
In this paper, silver nanoparticles are synthesized by using gelatin as the stabilizer, D-glucose (C6H12O6) as the deoxidizer and silver nitrate (AgNO3) as the precursor . The morphology, the particle size and its distribution can be featured with the help of ultraviolet visible spectrum(UV-vis), transmission electron microscope(TEM), X-ray diffraction(XRD). And the experimental results show that silver nanoparticles have spherical forms, the uniform particle size and the good dispersibility . The procedure is convenient and environmental, so it will have much significance and glorious prospect of application in the field of exploring the green synthetic methods.