西安工业大学学报
西安工業大學學報
서안공업대학학보
JOURNAL OF XI'AN TECHNOLOGICAL UNIVERSITY
2014年
4期
311-319
,共9页
郑琳%刘江南%高巍%要玉宏%王正品%党琦丹
鄭琳%劉江南%高巍%要玉宏%王正品%黨琦丹
정림%류강남%고외%요옥굉%왕정품%당기단
T92钢管%显微组织%析出相%力学性能%断裂机理
T92鋼管%顯微組織%析齣相%力學性能%斷裂機理
T92강관%현미조직%석출상%역학성능%단렬궤리
T92 steel tube%microstructure%precipitate%mechanical property%fracture mechanism
为了查明超超临界火力发电机组的高温锅炉管道T92耐热钢在高温长时服役过程中的组织及性能变化情况,通过光学显微观察、扫描电镜、EDS能谱分析、透射电镜分析、显微硬度测试,常规拉伸试验和微型杯突试验,研究了原始态及服役两年和三年的T92钢管的显微组织结构和力学性能的变化规律.试验结果表明:高温服役三年后的T92钢组织上仍然保持马氏体板条形态,析出碳化物的数量和尺寸不断增加,且服役两年及三年后组织中除了原始态时的M23C6和MX相,还在原奥氏体晶界及马氏体板条界处析出大量粗化较快的Laves相.材料室温力学性能随服役时间增加整体呈下降趋势,维氏硬度在服役三年后降低了13%,而其屈服强度,抗拉强度分别下降了5.35%和4.19%.SEM断口形貌分析可知随服役年限的增加,断裂特征由韧性断裂向韧脆混合断裂方式转变.
為瞭查明超超臨界火力髮電機組的高溫鍋爐管道T92耐熱鋼在高溫長時服役過程中的組織及性能變化情況,通過光學顯微觀察、掃描電鏡、EDS能譜分析、透射電鏡分析、顯微硬度測試,常規拉伸試驗和微型杯突試驗,研究瞭原始態及服役兩年和三年的T92鋼管的顯微組織結構和力學性能的變化規律.試驗結果錶明:高溫服役三年後的T92鋼組織上仍然保持馬氏體闆條形態,析齣碳化物的數量和呎吋不斷增加,且服役兩年及三年後組織中除瞭原始態時的M23C6和MX相,還在原奧氏體晶界及馬氏體闆條界處析齣大量粗化較快的Laves相.材料室溫力學性能隨服役時間增加整體呈下降趨勢,維氏硬度在服役三年後降低瞭13%,而其屈服彊度,抗拉彊度分彆下降瞭5.35%和4.19%.SEM斷口形貌分析可知隨服役年限的增加,斷裂特徵由韌性斷裂嚮韌脆混閤斷裂方式轉變.
위료사명초초림계화력발전궤조적고온과로관도T92내열강재고온장시복역과정중적조직급성능변화정황,통과광학현미관찰、소묘전경、EDS능보분석、투사전경분석、현미경도측시,상규랍신시험화미형배돌시험,연구료원시태급복역량년화삼년적T92강관적현미조직결구화역학성능적변화규률.시험결과표명:고온복역삼년후적T92강조직상잉연보지마씨체판조형태,석출탄화물적수량화척촌불단증가,차복역량년급삼년후조직중제료원시태시적M23C6화MX상,환재원오씨체정계급마씨체판조계처석출대량조화교쾌적Laves상.재료실온역학성능수복역시간증가정체정하강추세,유씨경도재복역삼년후강저료13%,이기굴복강도,항랍강도분별하강료5.35%화4.19%.SEM단구형모분석가지수복역년한적증가,단렬특정유인성단렬향인취혼합단렬방식전변.
T92 steel has become one of the main candidate alloys for ultra supercritical plants (USC) , therefore it is of great necessity to secure the safe service of generator set by exploring the rules behind the microstructure and mechanical property change under the condition of high temperature service . Metallographic microscopy , scanning electron microscopy , EDS analysis , transmission electron microscopy ,micro hardness test ,conventional tensile test and small punch test are conducted to measure the microstructure and mechanical properties of original state T 92 steel samples and the ones after two year and three year service .Results show :After three year service ,the microstructure of T92 steel still remains lath martensite ,but the number and size of the main precipitates have increased . Besides precipitates M23 C6 and MX ,which already exist in original T92 steel ,there is Laves phase particles emerging at the boundary of martensite and austenite in T 92 steel samples after two year service ,and the Laves phase experiences rapidly coarsening under high temperature service . Also ,the hardness ,yield strength and tensile strength decrease by 13% ,5 .35% and 4 .19% ,respectively .Meanwhile ,the SEM observation of instantaneous tensile fracture and small punch test fracture show s that the fracture has changed from the ductile fracture to ductile brittle fracture after serving .