农药科学与管理
農藥科學與管理
농약과학여관리
PESTICIDE SCIENCE AND ADMINISTRATION
2012年
1期
25-28
,共4页
吡虫啉%甲醇提取法%二氯甲烷提取法
吡蟲啉%甲醇提取法%二氯甲烷提取法
필충람%갑순제취법%이록갑완제취법
imidacloprid%extraction%dichloromethane%methanol
分别用二氯甲烷和甲醇提取小麦植株中的吡虫啉,添加回收率结果表明,甲醇提取吡虫啉添加回收率64.68~97.15%,低于二氯甲烷提取吡虫啉添加回收率102.25-105.24%;测定小麦中吡虫啉含量时二氯甲烷提取吡虫啉的量高于甲醇提取的量,为甲醇提取量的10-12倍:用二氯甲烷提取吡虫啉比甲醇提取吡虫啉操作简单,提取杂质少,可以作为小麦植株中吡虫啉提取的快速高效的溶剂。
分彆用二氯甲烷和甲醇提取小麥植株中的吡蟲啉,添加迴收率結果錶明,甲醇提取吡蟲啉添加迴收率64.68~97.15%,低于二氯甲烷提取吡蟲啉添加迴收率102.25-105.24%;測定小麥中吡蟲啉含量時二氯甲烷提取吡蟲啉的量高于甲醇提取的量,為甲醇提取量的10-12倍:用二氯甲烷提取吡蟲啉比甲醇提取吡蟲啉操作簡單,提取雜質少,可以作為小麥植株中吡蟲啉提取的快速高效的溶劑。
분별용이록갑완화갑순제취소맥식주중적필충람,첨가회수솔결과표명,갑순제취필충람첨가회수솔64.68~97.15%,저우이록갑완제취필충람첨가회수솔102.25-105.24%;측정소맥중필충람함량시이록갑완제취필충람적량고우갑순제취적량,위갑순제취량적10-12배:용이록갑완제취필충람비갑순제취필충람조작간단,제취잡질소,가이작위소맥식주중필충람제취적쾌속고효적용제。
A study on the comparation of dichloromethane and methanol for extraction of imidacloprid residues in wheat plants are carriedout.. The results show that the dichloromethane has higher extraction effect than that of methanol. The recoveries of dichloromethane extraction are 102.2%-105.2%, while the methanol are 64.68% - 97.15%. The imidacloprid residues detected in wheat extracted with dichloromethane are 10-12times higher than that of methanol. The extraction of imidacloprid with dichloromethane is simpler with fewer impurities than the extraction with methanol. Dichloromethane is an efficient extractant, for imidacloprid extraction from wheat.