中山大学学报(自然科学版)
中山大學學報(自然科學版)
중산대학학보(자연과학판)
ACTA SCIENTIARUM NATURALIUM UNIVERSITATIS SUNYATSENI
2014年
5期
88-91,97
,共5页
赵美峰%刘影%王建朝%胡博%陆军%黄严
趙美峰%劉影%王建朝%鬍博%陸軍%黃嚴
조미봉%류영%왕건조%호박%륙군%황엄
Tb-Fe-Co%化学镀%磁性能
Tb-Fe-Co%化學鍍%磁性能
Tb-Fe-Co%화학도%자성능
Tb-Fe-Co%electroless plating%magnetism
本文采用非水室温化学镀的方法制备了Tb-Fe-Co-B合金薄膜,并利用SEM、EDS、XRD和VSM分析了稀土Tb对镀层形貌、成分、结构和磁性能的影响。结果表明:稀土Tb的添加量在3 g/L时,镀层更趋于平整致密,镀速明显提高,而镀层结构并未有明显转变;但对镀层的饱和磁化率和矫顽力均有所提高。此外,通过600℃热处理可改变镀层的结构从而对合金的磁性产生较大的影响。
本文採用非水室溫化學鍍的方法製備瞭Tb-Fe-Co-B閤金薄膜,併利用SEM、EDS、XRD和VSM分析瞭稀土Tb對鍍層形貌、成分、結構和磁性能的影響。結果錶明:稀土Tb的添加量在3 g/L時,鍍層更趨于平整緻密,鍍速明顯提高,而鍍層結構併未有明顯轉變;但對鍍層的飽和磁化率和矯頑力均有所提高。此外,通過600℃熱處理可改變鍍層的結構從而對閤金的磁性產生較大的影響。
본문채용비수실온화학도적방법제비료Tb-Fe-Co-B합금박막,병이용SEM、EDS、XRD화VSM분석료희토Tb대도층형모、성분、결구화자성능적영향。결과표명:희토Tb적첨가량재3 g/L시,도층경추우평정치밀,도속명현제고,이도층결구병미유명현전변;단대도층적포화자화솔화교완력균유소제고。차외,통과600℃열처리가개변도층적결구종이대합금적자성산생교대적영향。
The Tb-Fe-Co-B thin films were prepared through a non-aqueous electroless plating method at room temperature.The structures and magnetic properties of Sm-Fe-Ni-B alloys were characterized using SEM,EDS,XRD and VSM analyses.The results indicated that the coating was smooth.The density, deposition rate were improved with 3 g/L of Tb solution.An amorphous of Fe-Co-B was changed with a microcrystalline state of Tb-Fe-Co-B.The saturation magnetization rate and coercivity were enhanced in the meantime.In addition,the structure could be changed to produce a greater effect on the magnetic al-loy at 600 ℃.