CAJ | 학술논문

采用溶胶一凝胶再结合程序升温溶剂热一步法制备了纳米复合光催化材料Ag-HeP2WtsOJTiO2，并采用傅立叶一红外光谱（FT-IR）、等离子原子反射光谱（ICP-AES）、氮气吸附一脱附测定和透射电子显微镜（TEM）等测试方法Ag-H6P2W18O62/TiO2合成材料的物理化学性质进行了表征。结果表明，复合材料中母体多酸的基本结构未发生明显变化，其Agl）J单质形式存在，且显示为介孔材料。在微波场作用下，复合材料Ag-H6P2W18O62/TiO2对甲基橙的降解表现了较高的催化活性。
채용용효일응효재결합정서승온용제열일보법제비료납미복합광최화재료Ag-HeP2WtsOJTiO2，병채용부립협일홍외광보（FT-IR）、등리자원자반사광보（ICP-AES）、담기흡부일탈부측정화투사전자현미경（TEM）등측시방법Ag-H6P2W18O62/TiO2합성재료적물이화학성질진행료표정。결과표명，복합재료중모체다산적기본결구미발생명현변화，기Agl）J단질형식존재，차현시위개공재료。재미파장작용하，복합재료Ag-H6P2W18O62/TiO2대갑기등적강해표현료교고적최화활성。
The nano-composite material Ag-H6P2W18O62/TiO2 in this study was prepared by sol-gel method combined with temperature-programmed hydrothermal treatment. The phase structures, chemical composition, opticalabsorption properties and surface physicochemical properties were characterized via FTIR, ICP-AES, XRD, nitrogen adsorption/desorption and TEM. The results showed the basic structure of polyoxometaltes in the composites has been basicly matained. The composites Ag-H6P2W18O62/TiO2 are periodical mesoporous materials, and the silver species existing in the nano-composite Ag-H6P2W18O62/TiO2 was metallic Ag. The photocatalytic activities of the as-prepared material were studied by the microwave assisted photodegradation of methyl orange. The results showed that the photocatalytic activitiy of Ag-H6P2W18O62/TiO2 for methyl orange was higher.