国际中医中药杂志
國際中醫中藥雜誌
국제중의중약잡지
INTERNATIONAL JOURNAL OF TRIDITIONAL CHINESE MEDICINE
2013年
9期
801-805
,共5页
刘洋%孙青%董红环%赵保胜%吕贝然%张雷%李智%杨文宁%隗丽
劉洋%孫青%董紅環%趙保勝%呂貝然%張雷%李智%楊文寧%隗麗
류양%손청%동홍배%조보성%려패연%장뢰%리지%양문저%외려
大豆%磷脂酰胆碱%制备工艺%质量控制
大豆%燐脂酰膽堿%製備工藝%質量控製
대두%린지선담감%제비공예%질량공제
Soybean%Phosphatidylcholine%Preparation process%Quality control
目的 研究大豆中磷脂酰胆碱的制备工艺.方法 ①先后采用氧化铝和安伯莱特XAD-2大孔树脂(Amberlite XAD-2 Macroporous Resin),运用柱色谱技术,从大豆中制备高纯磷脂酰胆碱；②以高效液相色谱法(High-performance liquid chromatography,HPLC)结合薄层色谱法(Thin layer chromatography,TLC)的方法,进行工艺过程分析和终产品质量控制.结果 建立了不同等级高纯大豆磷脂酰胆碱的制备工艺,并进行了定性定量质量控制.
目的 研究大豆中燐脂酰膽堿的製備工藝.方法 ①先後採用氧化鋁和安伯萊特XAD-2大孔樹脂(Amberlite XAD-2 Macroporous Resin),運用柱色譜技術,從大豆中製備高純燐脂酰膽堿；②以高效液相色譜法(High-performance liquid chromatography,HPLC)結閤薄層色譜法(Thin layer chromatography,TLC)的方法,進行工藝過程分析和終產品質量控製.結果 建立瞭不同等級高純大豆燐脂酰膽堿的製備工藝,併進行瞭定性定量質量控製.
목적 연구대두중린지선담감적제비공예.방법 ①선후채용양화려화안백래특XAD-2대공수지(Amberlite XAD-2 Macroporous Resin),운용주색보기술,종대두중제비고순린지선담감；②이고효액상색보법(High-performance liquid chromatography,HPLC)결합박층색보법(Thin layer chromatography,TLC)적방법,진행공예과정분석화종산품질량공제.결과 건립료불동등급고순대두린지선담감적제비공예,병진행료정성정량질량공제.
Objective To research the preparation process of soybean phosphatidylcholine.Methods ①the high purity soybean phosphatidylcholine was prepared with Al2O3 column chromatography and XAD-2resin column chromatography; ②combining methods of HPLC and TLC were used to control the process analysis and end products quality.Results The preparation process of different levels of high purity soybean phosphatidylcholine was setup up and qualitative and quantitative quality control was carried out.
