CAJ | 학술논문

对高效液相色谱一串联质谱法测定猪肉中磺胺多辛含量过程中引入的不确定度进行了分析和评定，通过试验计算出猪肉中磺胺多辛含量测量结果的不确定度。在置信水平为95％，包含因子k=2时，其相对扩展不确定度8．58％；当磺胺多辛含量为35．37μg／kg，其扩展不确定度为3．03μg／kg。样品的前处理所引入的不确定度对合成不确定度的贡献最大。
대고효액상색보일천련질보법측정저육중광알다신함량과정중인입적불학정도진행료분석화평정，통과시험계산출저육중광알다신함량측량결과적불학정도。재치신수평위95％，포함인자k=2시，기상대확전불학정도8．58％；당광알다신함량위35．37μg／kg，기확전불학정도위3．03μg／kg。양품적전처리소인입적불학정도대합성불학정도적공헌최대。
Uncertainties from the test results of sulfadoxine in pork by liquid chromatography tandem mass spectrometry were analyzed and assessed. The relative expended uncertainty calculated from the experimental date was 8.58% ,when the designed incredible probability was 95%(k=2). The expended uncertainty was 3.03 g / kg,while the content of sulfadoxine in the sample was 35.37 g / kg. The contribution of the uncertainty introduced by the sample pretreatment was the largest part to the combined uncertainty.