CAJ | 학술논문

目的：建立银杏叶片中9种大孔树脂有机溶剂残留物的检测方法。方法：采用顶空气相色谱法测定大孔树脂残留物正己烷、苯、甲苯、邻二甲苯、间二甲苯、对二甲苯、苯乙烯、二乙基苯和二乙烯苯的含量。结果：9种大孔树脂残留物得到较好的分离，呈良好线性关系（r为0.9992-0.9998），精密度良好，平均回收率为80%-110%。结论：该方法准确快捷，灵敏度高，适用于银杏叶片中树脂残留物的检查。
목적：건립은행협편중9충대공수지유궤용제잔류물적검측방법。방법：채용정공기상색보법측정대공수지잔류물정기완、분、갑분、린이갑분、간이갑분、대이갑분、분을희、이을기분화이을희분적함량。결과：9충대공수지잔류물득도교호적분리，정량호선성관계（r위0.9992-0.9998），정밀도량호，평균회수솔위80%-110%。결론：해방법준학쾌첩，령민도고，괄용우은행협편중수지잔류물적검사。
This study was aimed to establish the determination method of nineorganic solvent residues of macrop-orous resin. Headspace capillary gas chromatography (GC) was used in the content determination of hexane, benzene, methyl-benzene, o-xylene, m-xylene, p-xylene, styrene, diethyl-benzene and divinyl-benzene of macroporousresin residues in Ginkgo leaf tablets. The results showed that ninemacroporous resin residues in Ginkgo leaf tablets were completely separated. The calibration curves were in good linearity (r=0.9992-0.9998). The average recoveries were 80%-110%. It was concluded that themethod was accurate, quick, and sensitive, which can be used to determine the macroporous resin residues in Ginkgo leaf tablets.