广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2012年
12期
133-135
,共3页
罗爱嵘%佘金明%谢显珍%刘宏伟%肖玥
囉愛嶸%佘金明%謝顯珍%劉宏偉%肖玥
라애영%사금명%사현진%류굉위%초모
山苍子花蕾%挥发油%GC-MS分析
山蒼子花蕾%揮髮油%GC-MS分析
산창자화뢰%휘발유%GC-MS분석
flower buds of Litsea Cubeba%essential oil%GC-MS
通过水蒸汽蒸馏法提取山苍子花蕾挥发油,利用GC-MS联用技术对其成分进行定性定量分析。挥发油平均收率为3.8%,从中鉴定出40种成分,占总含量的87.27%。其中14个单萜烯烃化合物,占总含量的21.90%;12个单萜氧化物,占总含量的60.44%;12个倍半萜烯烃化合物,占总含量的4.85%。含量较高的成分为桉油精(39.86%)、松油醇(15.62%)、α-蒎烯(4.96%)、α-水芹烯(4.79%)。
通過水蒸汽蒸餾法提取山蒼子花蕾揮髮油,利用GC-MS聯用技術對其成分進行定性定量分析。揮髮油平均收率為3.8%,從中鑒定齣40種成分,佔總含量的87.27%。其中14箇單萜烯烴化閤物,佔總含量的21.90%;12箇單萜氧化物,佔總含量的60.44%;12箇倍半萜烯烴化閤物,佔總含量的4.85%。含量較高的成分為桉油精(39.86%)、鬆油醇(15.62%)、α-蒎烯(4.96%)、α-水芹烯(4.79%)。
통과수증기증류법제취산창자화뢰휘발유,이용GC-MS련용기술대기성분진행정성정량분석。휘발유평균수솔위3.8%,종중감정출40충성분,점총함량적87.27%。기중14개단첩희경화합물,점총함량적21.90%;12개단첩양화물,점총함량적60.44%;12개배반첩희경화합물,점총함량적4.85%。함량교고적성분위안유정(39.86%)、송유순(15.62%)、α-파희(4.96%)、α-수근희(4.79%)。
The essential oil in the flower buds of Litsea Cubeba was extracted by steam distillation,and the average extraction rate was 3.8%.Its components and relative contents were analyzed by gas chromatography-mass spectrometry(GC-MS),and 40 components in the oil were identified,which accounted for 87.27% of the total contents.There were 14 monoterpenes,which accounted for 21.90%,and 12 monoterpene oxides,accounted for 60.44%;and 12 sesquiterpenes,accounted for 4.85%.The main components were eucalyptol(39.86%),3-cyclohexene-1-methanol,alpha,alpha,4-trimethyl-,(S)-(15.62%),alpha pinene(4.96%),and alpha phellandrene(4.79%).