食品安全质量检测学报
食品安全質量檢測學報
식품안전질량검측학보
FOOD SAFETY AND QUALITY DETECTION TECHNOLOGY
2014年
9期
2657-2662
,共6页
何欢%王静文%李琼%罗中玉%曹进%王钢力%张庆生
何歡%王靜文%李瓊%囉中玉%曹進%王鋼力%張慶生
하환%왕정문%리경%라중옥%조진%왕강력%장경생
保健食品%离子迁移%非法添加
保健食品%離子遷移%非法添加
보건식품%리자천이%비법첨가
health foods%ion mobility spectrometry%illegal addition
目的:建立筛查保健食品中非法添加药物的新方法。方法对39种常见减肥类药物进行离子迁移(IMS)检测,建立该39种非法添加药物的IMS检测数据库。称取保健食品一次服用量,用无水乙醇溶解,取上清液点于试纸上,直接进样。通过离子迁移谱对减肥类保健食品中可能非法添加药物进行筛查。结果离子迁移测定39种可能非法添加的药物,其筛查的假阳性率小于10%,假阴性率小于5%。结论 IMS可以用于保健食品中非法添加药物的筛查,并具有较高的筛查效率,可作为保健食品监督检测中更快速、灵敏的技术手段。
目的:建立篩查保健食品中非法添加藥物的新方法。方法對39種常見減肥類藥物進行離子遷移(IMS)檢測,建立該39種非法添加藥物的IMS檢測數據庫。稱取保健食品一次服用量,用無水乙醇溶解,取上清液點于試紙上,直接進樣。通過離子遷移譜對減肥類保健食品中可能非法添加藥物進行篩查。結果離子遷移測定39種可能非法添加的藥物,其篩查的假暘性率小于10%,假陰性率小于5%。結論 IMS可以用于保健食品中非法添加藥物的篩查,併具有較高的篩查效率,可作為保健食品鑑督檢測中更快速、靈敏的技術手段。
목적:건립사사보건식품중비법첨가약물적신방법。방법대39충상견감비류약물진행리자천이(IMS)검측,건립해39충비법첨가약물적IMS검측수거고。칭취보건식품일차복용량,용무수을순용해,취상청액점우시지상,직접진양。통과리자천이보대감비류보건식품중가능비법첨가약물진행사사。결과리자천이측정39충가능비법첨가적약물,기사사적가양성솔소우10%,가음성솔소우5%。결론 IMS가이용우보건식품중비법첨가약물적사사,병구유교고적사사효솔,가작위보건식품감독검측중경쾌속、령민적기술수단。
Objective To establish a new method for screening chemicals illegally added in health foods. Methods Totally 39 kinds of common weight loss drugs were detected by ion mobility spectrometry (IMS) to establish IMS test database of 39 potential illegal addition chemicals. The sample was dissolved with ethanol, then dropped in test paper with the supernatant, after that detected directly. Ion mobility spectrometry was used to build a screening method for illegal addition in weight loss health foods. Results Totally 39 potential illegal addition chemicals were detected by IMS. The false positive ratio was below 10%as well as false negative ratio below 5%. Conclusion IMS can be used to screen the drugs illegal additions in healthy foods. It has relatively high screening efficiency, and can be regarded as a rapid and reliable technique in healthy foods supervision and inspection.