西部中医药
西部中醫藥
서부중의약
GANSU JOURNAL OF TRADITIONAL CHINESE MEDICINE
2014年
9期
43-45
,共3页
藏药六味能消散%没食子酸%理化鉴别%高效液相色谱法
藏藥六味能消散%沒食子痠%理化鑒彆%高效液相色譜法
장약륙미능소산%몰식자산%이화감별%고효액상색보법
Tibetan medicine LiuWei NengXiao powder%gallic acid%physical and chemical identification%HPLC
目的：建立藏药六味能消散质量标准。方法：对寒水石、碱花进行理化鉴别；用高效液相色谱法对没食子酸进行含量测定。结果：阴性对照无干扰；没食子酸在0.058～0.58μg范围内线性关系良好（r＝0.9999），平均加样回收率为98.1%，RSD=0.67%(n=6)。结论：本法简便、快速、结果准确可靠、专属性强、灵敏度高，可用于藏药六味能消散的质量控制。
目的：建立藏藥六味能消散質量標準。方法：對寒水石、堿花進行理化鑒彆；用高效液相色譜法對沒食子痠進行含量測定。結果：陰性對照無榦擾；沒食子痠在0.058～0.58μg範圍內線性關繫良好（r＝0.9999），平均加樣迴收率為98.1%，RSD=0.67%(n=6)。結論：本法簡便、快速、結果準確可靠、專屬性彊、靈敏度高，可用于藏藥六味能消散的質量控製。
목적：건립장약륙미능소산질량표준。방법：대한수석、감화진행이화감별；용고효액상색보법대몰식자산진행함량측정。결과：음성대조무간우；몰식자산재0.058～0.58μg범위내선성관계량호（r＝0.9999），평균가양회수솔위98.1%，RSD=0.67%(n=6)。결론：본법간편、쾌속、결과준학가고、전속성강、령민도고，가용우장약륙미능소산적질량공제。
Objective:To establish quality standard of Tibetan medicine LiuWei NengXiao powder. Methods:Gypsum and trona were identified from physical and chemical aspects;the contents of gallic acid were measured by HPLC. Results:It showed negative control and no interference;gallic acid presented good linear relationship in the range between 0.058 and 0.58 μg (r=0.999 9), average recovery rate was 98.1%, RSD=0.67%(n=6). Conclusion:The method is simple, rapid, accurate and reliable with strong specificity and high sensitivity, and it could be used for quality control of Tibetan medicine LiuWei NengXiao powder.
