石油化工腐蚀与防护
石油化工腐蝕與防護
석유화공부식여방호
PETROCHEMICAL CORROSION AND PROTECTION
2012年
5期
3-6
,共4页
彭松梓%崔新安%王春升%李春贤%郑晓鹏
彭鬆梓%崔新安%王春升%李春賢%鄭曉鵬
팽송재%최신안%왕춘승%리춘현%정효붕
静电聚结%绝缘电极%高含水乳化液%动态试验%原油脱水
靜電聚結%絕緣電極%高含水乳化液%動態試驗%原油脫水
정전취결%절연전겁%고함수유화액%동태시험%원유탈수
electrostatic coalescence%insulation electrode%high-water emulsion%dynamic test%crude oil dehydration
针对目前高含水原油采出液采用传统三相分离与热化学分离和电脱水方法存在分离级数和设备多、油水分离效率低、电脱水运行不稳定等问题,在静电预聚结研究基础上,采用自制绝缘电极和乳化液,开展静电聚结脱水研究,使水滴预聚结和沉降分离同时进行。通过静态聚结脱水试验考察了乳化液水含量、电压、温度和沉降时间等因素对静电聚结脱水效果的影响,结果表明乳化液脱水率随温度升高、电压增大和沉降时间延长而提高。其中温度影响最大,电压和沉降时间影响较小。在动态静电聚结原油脱水试验装置上进行验证,同时对不同分离器结构和不同电极结构及进料方式进行了对比,对试验条件进行了优化。动态试验结果表明,在电压2 kV,温度65~70℃,停留时间不大于10 min的条件下,高含水乳化液的脱水率均可达95%以上。
針對目前高含水原油採齣液採用傳統三相分離與熱化學分離和電脫水方法存在分離級數和設備多、油水分離效率低、電脫水運行不穩定等問題,在靜電預聚結研究基礎上,採用自製絕緣電極和乳化液,開展靜電聚結脫水研究,使水滴預聚結和沉降分離同時進行。通過靜態聚結脫水試驗攷察瞭乳化液水含量、電壓、溫度和沉降時間等因素對靜電聚結脫水效果的影響,結果錶明乳化液脫水率隨溫度升高、電壓增大和沉降時間延長而提高。其中溫度影響最大,電壓和沉降時間影響較小。在動態靜電聚結原油脫水試驗裝置上進行驗證,同時對不同分離器結構和不同電極結構及進料方式進行瞭對比,對試驗條件進行瞭優化。動態試驗結果錶明,在電壓2 kV,溫度65~70℃,停留時間不大于10 min的條件下,高含水乳化液的脫水率均可達95%以上。
침대목전고함수원유채출액채용전통삼상분리여열화학분리화전탈수방법존재분리급수화설비다、유수분리효솔저、전탈수운행불은정등문제,재정전예취결연구기출상,채용자제절연전겁화유화액,개전정전취결탈수연구,사수적예취결화침강분리동시진행。통과정태취결탈수시험고찰료유화액수함량、전압、온도화침강시간등인소대정전취결탈수효과적영향,결과표명유화액탈수솔수온도승고、전압증대화침강시간연장이제고。기중온도영향최대,전압화침강시간영향교소。재동태정전취결원유탈수시험장치상진행험증,동시대불동분리기결구화불동전겁결구급진료방식진행료대비,대시험조건진행료우화。동태시험결과표명,재전압2 kV,온도65~70℃,정류시간불대우10 min적조건하,고함수유화액적탈수솔균가체95%이상。
To solve the problems of numerous separation stages,more equipment,lower separation efficiency and unstable running of electric dehydration in conventional separation process of three phase separation,thermal chemistry separation and electric dehydration treatment,researches on electrostatic coalescence for high water content oil is developed based on the former studies on pre-coalescence by using complex electrode and emulsion made in laboratory.The impacts of water content of emulsion,electric voltage,temperature and residence time etc on the dehydration performance of emulsion by electrostatic coalescence were investigated through static experiments and were then validated and optimized through the dynamic experiments.The results show that the dehydration rate of emulsion increases with increase of temperature,voltage and residence time.In these impact factors,temperature has the greatest impact,followed by voltage and residence time.At the same time,the different separator constructions,different electrode structures and different feedings are compared and testing conditions are optimized.The dynamic experiments results demonstrate that,under the conditions of 2 000 V voltage,65~70 ℃ temperature and the maximum resident time of 10 minutes,the dehydration rate is over 95%.