现代农药
現代農藥
현대농약
MODERN AGROCHEMICALS
2014年
2期
30-32
,共3页
吕印美%李晓红%李太衬%姚刚%王肖
呂印美%李曉紅%李太襯%姚剛%王肖
려인미%리효홍%리태츤%요강%왕초
醚菌酯%啶酰菌胺%高效液相色谱%分析
醚菌酯%啶酰菌胺%高效液相色譜%分析
미균지%정선균알%고효액상색보%분석
kresoxim-methyl%boscalid%HPLC%analysis
采用高效液相色谱法，以甲醇和水为流动相，经C18色谱柱分离，在230 nm下同时定量测定30%醚菌·啶酰菌悬浮剂各有效成分含量。结果表明：醚菌酯和啶酰菌胺的线性相关系数分别为0.9999、0.9998，标准偏差分别为0.070、0.095，变异系数分别为0.70%、0.47%，平均回收率分别为99.65%、99.52%。此分析方法分析快速，结果可信度高，适用于农药制剂产品中啶酰菌胺和醚菌酯有效成分的质量分析。
採用高效液相色譜法，以甲醇和水為流動相，經C18色譜柱分離，在230 nm下同時定量測定30%醚菌·啶酰菌懸浮劑各有效成分含量。結果錶明：醚菌酯和啶酰菌胺的線性相關繫數分彆為0.9999、0.9998，標準偏差分彆為0.070、0.095，變異繫數分彆為0.70%、0.47%，平均迴收率分彆為99.65%、99.52%。此分析方法分析快速，結果可信度高，適用于農藥製劑產品中啶酰菌胺和醚菌酯有效成分的質量分析。
채용고효액상색보법，이갑순화수위류동상，경C18색보주분리，재230 nm하동시정량측정30%미균·정선균현부제각유효성분함량。결과표명：미균지화정선균알적선성상관계수분별위0.9999、0.9998，표준편차분별위0.070、0.095，변이계수분별위0.70%、0.47%，평균회수솔분별위99.65%、99.52%。차분석방법분석쾌속，결과가신도고，괄용우농약제제산품중정선균알화미균지유효성분적질량분석。
A method was established for determination of kresoxim-methyl and boscalid in 30%SC by HPLC using C18 column with DAD detector at 230 nm, methanol and water (volume ratio of 70︰30) as mobile phase. The results showed that the linear correlation coefficients of kresoxim-methyl and boscalid were 0.999 9 and 0.999 8, the standard deviations were 0.070 and 0.095, the variation coefficients were 0.70% and 0.47%, and the average recoveries were 99.65% and 99.52%, respectively.
