山东化工
山東化工
산동화공
SHANDONG CHEMICAL INDUSTRY
2012年
3期
43-46
,共4页
氧化锌%纳米棒%固态合成%低温%表征
氧化鋅%納米棒%固態閤成%低溫%錶徵
양화자%납미봉%고태합성%저온%표정
zinc oxide%nanorod%solid - state synthesis%low temperature%characterization
以无水ZnSO4与NaOH为原料，在红外灯照射下，通过低温固态化学反应路线制备ZnO纳米棒。通过XRD、XPS和TEM对制得的ZnO纳米棒的结构和形貌进行了分析。研究表明产物的形貌和尺寸可通过调节实验条件（如原料比、有无照射、盐的类型等）加以控制。
以無水ZnSO4與NaOH為原料，在紅外燈照射下，通過低溫固態化學反應路線製備ZnO納米棒。通過XRD、XPS和TEM對製得的ZnO納米棒的結構和形貌進行瞭分析。研究錶明產物的形貌和呎吋可通過調節實驗條件（如原料比、有無照射、鹽的類型等）加以控製。
이무수ZnSO4여NaOH위원료，재홍외등조사하，통과저온고태화학반응로선제비ZnO납미봉。통과XRD、XPS화TEM대제득적ZnO납미봉적결구화형모진행료분석。연구표명산물적형모화척촌가통과조절실험조건（여원료비、유무조사、염적류형등）가이공제。
ZnO nanorods had been synthesized via a solid -state reaction route between anhydrous ZnSO4 and NaOH under the irradiation of the 250 W IR lamp at relatively low temperature. The structure and shape of ZnO nanorods were analysed by XRD, XPS and TEM. The results showed that the size and morphology of the resulted products could be controlled through adjusting the reaction conditions, including Zn2＋/OH-ratio,with and without the irradiation of IR lamp and the kind of zinc salt.
