CAJ | 학술논문

研究了在Pd/C催化下水合肼还原对硝基苯乙酸制备对氨基苯乙酸的方法．讨论了反应时间、反应温度、水合肼及催化剂用量对产物收率的影响，在优化条件下对氨基苯乙酸的收率达89.52％．经IR 、MS和NMR证实了其结构．
연구료재Pd/C최화하수합정환원대초기분을산제비대안기분을산적방법．토론료반응시간、반응온도、수합정급최화제용량대산물수솔적영향，재우화조건하대안기분을산적수솔체89.52％．경IR 、MS화NMR증실료기결구．
The preparation method of 4-aminophenylacetic acid by reduction of 4-nitrophenylacetic acid with hydrazine hydrate in presence of Pd/C catalyst was studied .The influences on the product yield of reaction time , reaction temperature and quantities of hydrazine hydrate and catalyst used were investigated .Under the optimum conditions ,the yield of 4-aminophenylacetic acid could reach 89.52% . IR and 1 HNMR proved the structure of product .