中国药师
中國藥師
중국약사
CHINA PHARMACIST
2014年
5期
737-739,740
,共4页
唐勇琛%梁学政%吕建伟%徐宏%甄汉深%丘琴%关君霞
唐勇琛%樑學政%呂建偉%徐宏%甄漢深%丘琴%關君霞
당용침%량학정%려건위%서굉%견한심%구금%관군하
益水生新饮颗粒%马钱苷%高效液相色谱%薄层色谱%质量标准
益水生新飲顆粒%馬錢苷%高效液相色譜%薄層色譜%質量標準
익수생신음과립%마전감%고효액상색보%박층색보%질량표준
Yishui Shengxinyin granules%Loganin%HPLC%TLC%Quality standard
目的：建立益水生新饮颗粒的质量标准。方法：采用薄层色谱法对方中山茱萸、熟地黄、山药进行定性鉴别；采用高效液相色谱法测定马钱苷的含量。结果：TLC斑点清晰,阴性对照无干扰；马钱苷的进样量在0.112~1.120μg范围内与峰面积呈良好的线性(r=0.9995),平均回收率为100.02%,RSD为1.96%(n=6)。结论：鉴别方法专属性强,定量方法准确可靠,所建标准可用于益水生新饮颗粒的质量控制。
目的：建立益水生新飲顆粒的質量標準。方法：採用薄層色譜法對方中山茱萸、熟地黃、山藥進行定性鑒彆；採用高效液相色譜法測定馬錢苷的含量。結果：TLC斑點清晰,陰性對照無榦擾；馬錢苷的進樣量在0.112~1.120μg範圍內與峰麵積呈良好的線性(r=0.9995),平均迴收率為100.02%,RSD為1.96%(n=6)。結論：鑒彆方法專屬性彊,定量方法準確可靠,所建標準可用于益水生新飲顆粒的質量控製。
목적：건립익수생신음과립적질량표준。방법：채용박층색보법대방중산수유、숙지황、산약진행정성감별；채용고효액상색보법측정마전감적함량。결과：TLC반점청석,음성대조무간우；마전감적진양량재0.112~1.120μg범위내여봉면적정량호적선성(r=0.9995),평균회수솔위100.02%,RSD위1.96%(n=6)。결론：감별방법전속성강,정량방법준학가고,소건표준가용우익수생신음과립적질량공제。
Objective:To establish the quality standard for Yishui Shengxinyin granules. Methods: Qualitative identification of Cornus officinalis, Rehmannia glutinosa and Dioscorea opposita was conducted by TLC. The content of loganin was determined by HPLC. Results:TLC spots were clear without interference from negative sample. The linear range of loganin was 0. 112-1. 120μg(r=0. 999 5)with the average recovery of 100. 02%(RSD=1. 96%, n=6). Conclusion:The established quality standard can be used in the quality control of Yishui Shengxinyin granules.
