热带农业科学
熱帶農業科學
열대농업과학
CHINESE JOURNAL OF TROPICAL AGRICULTURE
2012年
11期
87-89,96
,共4页
何秀芬%陈歆%张瑞芳%汤建彪
何秀芬%陳歆%張瑞芳%湯建彪
하수분%진흠%장서방%탕건표
离子色谱%剑麻叶%氯离子%测定
離子色譜%劍痳葉%氯離子%測定
리자색보%검마협%록리자%측정
ion chromatography%sisal leaves%chlorine%determination
提出离子色谱法测定剑麻叶中氯离子的方法:剑麻叶样品在超声波振荡条件下用水进行浸提,经炭黑小柱对提取的水溶液进行净化之后,采用离子色谱测定。经大批样品的实验测定结果证明,本方法平均回收率在95%~106%,RSD小于0.45%。该方法具有简单、重复性好、灵敏度高、准确性好等较多优点,适用于剑麻样品分析。
提齣離子色譜法測定劍痳葉中氯離子的方法:劍痳葉樣品在超聲波振盪條件下用水進行浸提,經炭黑小柱對提取的水溶液進行淨化之後,採用離子色譜測定。經大批樣品的實驗測定結果證明,本方法平均迴收率在95%~106%,RSD小于0.45%。該方法具有簡單、重複性好、靈敏度高、準確性好等較多優點,適用于劍痳樣品分析。
제출리자색보법측정검마협중록리자적방법:검마협양품재초성파진탕조건하용수진행침제,경탄흑소주대제취적수용액진행정화지후,채용리자색보측정。경대비양품적실험측정결과증명,본방법평균회수솔재95%~106%,RSD소우0.45%。해방법구유간단、중복성호、령민도고、준학성호등교다우점,괄용우검마양품분석。
A method for the determination of chlorine (C1-) in sisal leaves was established with ion chromatography. The sample was extracted with water by ultrasonic method, and purified by SPE on carbon black micro-column, then determined with ion chromatography. Tests for recovery and precision were made, giving values of recovery ranged from 95%-106%, RSD was less than 0.45%. The method is simple, accurate, stable and precise. It can be easily and conveniently adopted for the routine quality control analysis.