CAJ | 학술논문

紫外光固化引发剂是光固化技术的核心组成，用量少，但对反应的性能起着关键作用。光固化引发剂JD102（化学名称：1-[4-（2-羟乙氧基）苯基]2-羟基-2-甲基-1-丙酮）具有低气味、耐黄变形好、透明性佳、抗氧化阻聚、可水溶、符合FDA认证的优点，广泛用于UV油墨、木器涂料、光学等高端领域。本文以乙二醇苯醚醋酸酯和异丁酰氯为原料，通过对传统合成工艺的改进，使反应简捷，同时采用相转移催化技术，使反应效率更高、环保性更好地合成出紫外光固化引发剂JD102，并成功进行了产业化。
자외광고화인발제시광고화기술적핵심조성，용량소，단대반응적성능기착관건작용。광고화인발제JD102（화학명칭：1-[4-（2-간을양기）분기]2-간기-2-갑기-1-병동）구유저기미、내황변형호、투명성가、항양화조취、가수용、부합FDA인증적우점，엄범용우UV유묵、목기도료、광학등고단영역。본문이을이순분미작산지화이정선록위원료，통과대전통합성공예적개진，사반응간첩，동시채용상전이최화기술，사반응효솔경고、배보성경호지합성출자외광고화인발제JD102，병성공진행료산업화。
UV-curing photo initiator is a core part of UV-curing technology, it plays an important role in reaction with little amount. UV-curing photo initiator JD102 (chemical name: 1-[4-(2-Hydroxyethoxy- phenyl)]2-hydroxy-2-methyl-l-propane) is widely used in UV-inks, UV-wood paints, optical fields due to its excellent properties of low odor, non-yellowing, good transparency, oxygen inhibition-resisting, water solubility, it fit to the requirement of FDA. UV-curing photo initiator JDI02 was synthesized by using ethylene glycol phenyl ether acetate and butyl chloride as raw materials, by improvement of the traditional process and using phase transfer catalysis technology, the efficiency higher than traditional process, it is a better environment friendlv and simply reaction and successful achieved industrialization.