江苏科技大学学报(自然科学版)
江囌科技大學學報(自然科學版)
강소과기대학학보(자연과학판)
JOURNAL OF JIANGSU UNIVERSITY OF SCIENCE AND TECHNOLOGY(NATURAL SCIENCE EDITION)
2013年
4期
342-346
,共5页
高延敏%杜财钢%代仕梅%吴欣凯
高延敏%杜財鋼%代仕梅%吳訢凱
고연민%두재강%대사매%오흔개
PANI/CuFeS2%复合材料%原位聚合法%包覆
PANI/CuFeS2%複閤材料%原位聚閤法%包覆
PANI/CuFeS2%복합재료%원위취합법%포복
PANI/CuFeS2%composite material%in-situ polymerization%covered
聚苯胺/CuFeS2(PANI/CuFeS2)纳米复合材料不仅具有导电高聚物和氧化物半导体的优良光电特性,还具有纳米材料特有的功能性,在传感、催化、吸波和能源材料等领域有着广阔的应用前景。文中采用原位聚合法制备了PANI/CuFeS2纳米复合材料,分别采用傅立叶红外光谱(FT-IR)、X-射线衍射(XRD)、扫描电镜(SEM)、UV-Vis 漫反射吸收光谱和电导率测量等对所得复合微粒进行表征。结果表明:CuFeS2纳米颗粒均匀的分散在聚苯胺( PANI)基体内,PANI/CuFeS2复合材料中未存在键合作用,而只是简单的物理包覆,所以对各自的性能均未造成影响。与聚苯胺相比,PANI/CuFeS2复合材料光电性能得到有效提高,且CuFeS 2添加量为30%时其性能最佳。
聚苯胺/CuFeS2(PANI/CuFeS2)納米複閤材料不僅具有導電高聚物和氧化物半導體的優良光電特性,還具有納米材料特有的功能性,在傳感、催化、吸波和能源材料等領域有著廣闊的應用前景。文中採用原位聚閤法製備瞭PANI/CuFeS2納米複閤材料,分彆採用傅立葉紅外光譜(FT-IR)、X-射線衍射(XRD)、掃描電鏡(SEM)、UV-Vis 漫反射吸收光譜和電導率測量等對所得複閤微粒進行錶徵。結果錶明:CuFeS2納米顆粒均勻的分散在聚苯胺( PANI)基體內,PANI/CuFeS2複閤材料中未存在鍵閤作用,而隻是簡單的物理包覆,所以對各自的性能均未造成影響。與聚苯胺相比,PANI/CuFeS2複閤材料光電性能得到有效提高,且CuFeS 2添加量為30%時其性能最佳。
취분알/CuFeS2(PANI/CuFeS2)납미복합재료불부구유도전고취물화양화물반도체적우량광전특성,환구유납미재료특유적공능성,재전감、최화、흡파화능원재료등영역유착엄활적응용전경。문중채용원위취합법제비료PANI/CuFeS2납미복합재료,분별채용부립협홍외광보(FT-IR)、X-사선연사(XRD)、소묘전경(SEM)、UV-Vis 만반사흡수광보화전도솔측량등대소득복합미립진행표정。결과표명:CuFeS2납미과립균균적분산재취분알( PANI)기체내,PANI/CuFeS2복합재료중미존재건합작용,이지시간단적물리포복,소이대각자적성능균미조성영향。여취분알상비,PANI/CuFeS2복합재료광전성능득도유효제고,차CuFeS 2첨가량위30%시기성능최가。
Apart from perfect optical and electrical characteristics of both conducting polymers and oxide semi-conductors, PANI/CuFeS2 nano composite also has unique functionality of nano materials , so it could be widely used in fields such as sense , catalysis, microwave absorbing and energy materials .The PANI/CuFeS2 nano com-posite was prepared by in-situ polymerization , these composite particles were characterized by FT -IR, XRD, UV-Vis, SEM, conductivity measurement .The main research results obtained are as follows: CuFeS2 nano-particles were dispersed in polyaniline matrix and covered simply , functive key did not exist in PANI/CuFeS2 composite materials , so their performances were not affected .Compared with polyaniline , the photoelectric prop-erty of PANI/CuFeS2 composite could be improved effectively , and the photoelectric property was the best when the addition of CuFeS 2 was 30%.