广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2012年
23期
99-102
,共4页
果蔬%重金属%ICP%评价
果蔬%重金屬%ICP%評價
과소%중금속%ICP%평개
vegetable%heavy metal%ICP%evaluation
以8种果蔬(9种样品)为研究对象,采用湿法消解,建立了ICP—AES同时检测铜、钴、镍、铬、镉和铅六种重金属元素含量的测定方法。在最优条件下,实验结果表明:Cu、Pb、Ni、Cr、Cd和Co的检出限分别为0.0015μg·mL^-1、0.024μg·mL^-1、0.0042μg·mL^-1、0.0033txg·mL^-1、0.0006μg·mL^-1和0.0021Ixg·mL^-1,相对标准偏差介于0.12%^-110.29%之间,加标回收实验中回收率均介于89.4%-108.6%之间(土豆中Ni的回收率为123.7%)。根据国家食品卫生标准中的果蔬类标准,通过分析得出,Cr、Cd两种重金属元素污染比较严重,对居民的身体健康存在潜在的威胁。
以8種果蔬(9種樣品)為研究對象,採用濕法消解,建立瞭ICP—AES同時檢測銅、鈷、鎳、鉻、鎘和鉛六種重金屬元素含量的測定方法。在最優條件下,實驗結果錶明:Cu、Pb、Ni、Cr、Cd和Co的檢齣限分彆為0.0015μg·mL^-1、0.024μg·mL^-1、0.0042μg·mL^-1、0.0033txg·mL^-1、0.0006μg·mL^-1和0.0021Ixg·mL^-1,相對標準偏差介于0.12%^-110.29%之間,加標迴收實驗中迴收率均介于89.4%-108.6%之間(土豆中Ni的迴收率為123.7%)。根據國傢食品衛生標準中的果蔬類標準,通過分析得齣,Cr、Cd兩種重金屬元素汙染比較嚴重,對居民的身體健康存在潛在的威脅。
이8충과소(9충양품)위연구대상,채용습법소해,건립료ICP—AES동시검측동、고、얼、락、력화연륙충중금속원소함량적측정방법。재최우조건하,실험결과표명:Cu、Pb、Ni、Cr、Cd화Co적검출한분별위0.0015μg·mL^-1、0.024μg·mL^-1、0.0042μg·mL^-1、0.0033txg·mL^-1、0.0006μg·mL^-1화0.0021Ixg·mL^-1,상대표준편차개우0.12%^-110.29%지간,가표회수실험중회수솔균개우89.4%-108.6%지간(토두중Ni적회수솔위123.7%)。근거국가식품위생표준중적과소류표준,통과분석득출,Cr、Cd량충중금속원소오염비교엄중,대거민적신체건강존재잠재적위협。
Eight kinds of fruits and vegetables ( nine kinds of sample) as the research objects, using wet digestion, a method of simultaneous detection of the concentration of six heavy elements Cu, Pb, Ni, Cr, Cd, and Co using ICP-AES was established. Under optimal conditions, the experimental results showed that the detection limits of Cu, Pb, Ni, Cr, Cd and Co were 0. 0015 μg · mL^-1 , 0. 024 μg - mL^-1 , 0. 0042 μg · mL^-1 , 0. 0033 μg · mL^-1 , 0. 0006 μg · mL-land 0. 0021 μg · mL^-1 respectively. Relative standard deviation was between 0. 12% and 10. 29% , recoveries ranged from 89.4% to 108.6% ( the recovery of Ni in potatoes was 123.7% ). According to the national food hygiene standards in the fruit and vegetable standards, the results showed that pollution was more serious of the two heavy metal el- ements Cr and Cd, causing a potential threat to the physical health of the residents.