CAJ | 학술논문

采用高效液相色谱法，以甲醇-乙腈-水（体积比为50：40：10，加入0．01％三乙胺）为流动相，使用C18反相柱和紫外可变波长检测器（波长245nm），用外标法对15％甲维刈比虫啉悬浮剂进行了定量分析。结果表明，方法中甲维盐和吡虫啉标准偏差分别为0．04，0．05，变异系数分别为0．77％，0．49％，平均回收率分别为99．07％，100．04％。
채용고효액상색보법，이갑순-을정-수（체적비위50：40：10，가입0．01％삼을알）위류동상，사용C18반상주화자외가변파장검측기（파장245nm），용외표법대15％갑유예비충람현부제진행료정량분석。결과표명，방법중갑유염화필충람표준편차분별위0．04，0．05，변이계수분별위0．77％，0．49％，평균회수솔분별위99．07％，100．04％。
A method was developed for the analysis of 15 % suspension concentrate formulation of emamectin benzo-ate and imidacloprid by high-performance liquid chromatography (HPLC) on ClS column with UV-absorbance detector (wavelength 245 nm) and mobile phase of methanol- acetonitrile-water (volume ratio of 50:40 : 10, adding 0.01% triethylamine). The results showed that the standard deviations, variation coefficients and average recoveries of emamectin benzoate and imidacloprid were 0. 04, 0. 77% , 99.07% and 0. 05, 0. 49% , 100. 04% , respectively.