CAJ | 학술논문

采用GB／T24893--2010（（动植物油脂多环芳烃的测定》中的液液萃取方法提取动植物油脂中的苯并（a）芘，用中性氧化铝固相萃取柱净化，用反相高效液相色谱法-荧光检测器定量检测试样中的苯并（a）芘含量。实验结果表明植物油的平均加标回收率为91．44％，动物油的平均加标回收率为91．69％。以茶油为试样，测定结果的相对标准偏差（RSD）为1．48％（n=7）。改进方法简单、操作易控制、方法精密度好、回收率高，适合测定动植物油脂中的苯并（a）芘含量。
채용GB／T24893--2010（（동식물유지다배방경적측정》중적액액췌취방법제취동식물유지중적분병（a）비，용중성양화려고상췌취주정화，용반상고효액상색보법-형광검측기정량검측시양중적분병（a）비함량。실험결과표명식물유적평균가표회수솔위91．44％，동물유적평균가표회수솔위91．69％。이다유위시양，측정결과적상대표준편차（RSD）위1．48％（n=7）。개진방법간단、조작역공제、방법정밀도호、회수솔고，괄합측정동식물유지중적분병（a）비함량。
The benzo(a) pyrene was extracted from animal and vegetable fats and oils by liquid phase ex- traction according to GB/T 24893 - 2010 Animal and vegetable fats and oils - Determination of polycyclic aromatic hydrocarbons, which was purified by solid phase extraction of neutral alumina column, and de- termined by reverse -phase high performance liquid chromatography - fluorescence method. The results indicated that the average recovery rate for vegetable fats and oils was 91.44%, and that for animal fats and oils was 91.69%. The relative standard deviation was 1.48% (n = 7 )for the determination results of tea seed oil. This revised method was simple and easy to operate, had good precision and high rate of re- coveries. Thus the revised method was fit for determination of benzo(a) pyrene content in animal and veg- etable fats and oils.