生物质化学工程
生物質化學工程
생물질화학공정
BIOMASS CHEMICAL ENGINEERING
2012年
6期
12-16
,共5页
张宗和%闵凡芹%秦清%徐浩%李文君%王成章
張宗和%閔凡芹%秦清%徐浩%李文君%王成章
장종화%민범근%진청%서호%리문군%왕성장
五倍子%单宁酸%响应面法%提取%超声波
五倍子%單寧痠%響應麵法%提取%超聲波
오배자%단저산%향응면법%제취%초성파
Chinese gallnut%tannic acid%response surface method%exaction%ultrasonic
以水为提取溶剂,在单因素试验的基础上,利用响应面分析法优化了五倍子中单宁酸的超声波辅助提取条件。利用中心组合(Box—Behnken)实验设计原理研究液固比、超声波作用时间、超声波功率3个自变量对响应值单宁酸提取得率的影响。结果表明,单宁酸最佳超声波辅助提取条件为:5g五倍子粉末,液固比38:1(mL:g),超声波提取时间32min,超声波功率250w,在此条件下单宁酸提取得率为66.0%。
以水為提取溶劑,在單因素試驗的基礎上,利用響應麵分析法優化瞭五倍子中單寧痠的超聲波輔助提取條件。利用中心組閤(Box—Behnken)實驗設計原理研究液固比、超聲波作用時間、超聲波功率3箇自變量對響應值單寧痠提取得率的影響。結果錶明,單寧痠最佳超聲波輔助提取條件為:5g五倍子粉末,液固比38:1(mL:g),超聲波提取時間32min,超聲波功率250w,在此條件下單寧痠提取得率為66.0%。
이수위제취용제,재단인소시험적기출상,이용향응면분석법우화료오배자중단저산적초성파보조제취조건。이용중심조합(Box—Behnken)실험설계원리연구액고비、초성파작용시간、초성파공솔3개자변량대향응치단저산제취득솔적영향。결과표명,단저산최가초성파보조제취조건위:5g오배자분말,액고비38:1(mL:g),초성파제취시간32min,초성파공솔250w,재차조건하단저산제취득솔위66.0%。
The ultrasonic-assisted extraction of tannic acid from Chinese gallnut with water as extraction agent were determined on the basis of single factor experiment using response surface method ( RSM ). According to central composite ( Box-Behnken ) design principle, the effect of three independent variables on the Yield of tannic acid, namely liquid to solid ratio, ultrasonic extraction time, and ultrasonic power was investigated. The results showed the optimum ultrasonic-assisted extraction conditions were: 5 g of Chinese gallnut powder, liquid to solid ratio 38 : 1 ( mL: g), ultrasonic extraction time 32 min, ultrasonic power 250 W. Under the optimum conditions, the extraction yield of tannic acid was 66.0 %.