广东化工
廣東化工
엄동화공
GUANGDONG CHEMICAL INDUSTRY
2012年
15期
66-67,69
,共3页
纳米纤维索%竹浆%超声辅助%响应面法优化
納米纖維索%竹漿%超聲輔助%響應麵法優化
납미섬유색%죽장%초성보조%향응면법우화
nano-cellulose: bamboo pulp%ultrasound-assisted: response surface methodology optimization
响应面法优化超声波辅助酸水解制备竹浆纳米纤维素工艺条件，结果表明纳米纤维素优化制备工艺条件为超声时间22min，反应温度49．46℃，反应时间3．25h。优化条件下纳米纤维素得率平均为49．92％，与响应面法纳米纤维素得率预测值50．08％相接近。影响纳米纤维素得率的因素依次为反应时间、超声时间和反应温度。
響應麵法優化超聲波輔助痠水解製備竹漿納米纖維素工藝條件，結果錶明納米纖維素優化製備工藝條件為超聲時間22min，反應溫度49．46℃，反應時間3．25h。優化條件下納米纖維素得率平均為49．92％，與響應麵法納米纖維素得率預測值50．08％相接近。影響納米纖維素得率的因素依次為反應時間、超聲時間和反應溫度。
향응면법우화초성파보조산수해제비죽장납미섬유소공예조건，결과표명납미섬유소우화제비공예조건위초성시간22min，반응온도49．46℃，반응시간3．25h。우화조건하납미섬유소득솔평균위49．92％，여향응면법납미섬유소득솔예측치50．08％상접근。영향납미섬유소득솔적인소의차위반응시간、초성시간화반응온도。
Ultrasound-assisted acid hydrolysis preparation technological conditions of bamboo pulp nano-cellulose were optimized by response surface methodology. The results showed that optimization of nano-cellulose preparation technological conditions was 22 min of ultrasound time, 49.46℃ of reaction temperature and 3.25 h of reaction time. Under optimization, nano-cellulose average yield was 49.92 %, which was closed to 50.08 % of response surface methodology predicted values. The influencing factors of nano-cellulose yield are followed by reaction time, ultrasound time and reaction temperature.
