广东化工
廣東化工
엄동화공
GUANGDONG CHEMICAL INDUSTRY
2012年
16期
25-26
,共2页
牛肝菌%提取%研究
牛肝菌%提取%研究
우간균%제취%연구
polysaccharide%xerocomus: extraction%research
本篇研究了牛肝菌中多糖的最佳提取工艺。考虑到料水比对多糖得率的影响最小,且浸挺过程中若料水比过大,则浸出液也就相应增多,为了减轻浓缩等后处理工艺的负担,根据正交实验设计优化:温度80℃,料水比1:15(g/mL)、提取时间3h,乙醇浓度85%为最适工艺,此条件下多糖的得率为5.0%。经初步纯化得到纯度为48%粗多糖。
本篇研究瞭牛肝菌中多糖的最佳提取工藝。攷慮到料水比對多糖得率的影響最小,且浸挺過程中若料水比過大,則浸齣液也就相應增多,為瞭減輕濃縮等後處理工藝的負擔,根據正交實驗設計優化:溫度80℃,料水比1:15(g/mL)、提取時間3h,乙醇濃度85%為最適工藝,此條件下多糖的得率為5.0%。經初步純化得到純度為48%粗多糖。
본편연구료우간균중다당적최가제취공예。고필도료수비대다당득솔적영향최소,차침정과정중약료수비과대,칙침출액야취상응증다,위료감경농축등후처리공예적부담,근거정교실험설계우화:온도80℃,료수비1:15(g/mL)、제취시간3h,을순농도85%위최괄공예,차조건하다당적득솔위5.0%。경초보순화득도순도위48%조다당。
The paper researched the best extraction technology of polysaccharide from Xerocomus. In consideration of the minimum influence to material water ratio of polysaccharides, and in the process of leaching, if the ratio of material to water oversize, then the leaching liquid will increase corresponding. In order to reduce the technologic burden after enrichment processing, according to the orthogonal experimental design optimization: temperature 80℃, the ratio of material to water 1:15 (g/mL), extracting time 3 h, ethanol concentration 85 %. In this condition, polysaccharide yield was 5.0 %. After basic purification, we can get the purity was 48 % of coarse polysaccharide.